Synthesis and Application of Sol-Gel-Derived Nano-Silica in Glass Ionomer Cement for Dental Cementation.

Although glass ionomer cements (GIC) are widely used in dental restorations, their long-term performance remains limited by their mechanical properties, including surface roughness and fracture resistance. This study investigates the synthesis of nano-silica from sp. diatoms through the sol-gel process and its application in influencing the mechanical and physical properties of GIC luting materials. A control group and three experimental groups of different nano-silica concentrations (1%, 3%, and 5%) were compared. Several analyses, including confocal laser scanning microscopy (CLSM), scanning electron microscopy (SEM), and universal testing machines (UTM), were used to determine layer thickness, surface roughness, compressive strength, and tensile strength. Statistical analysis exhibited significant differences between the groups ( < 0.05). The 3% nano-silica group indicated an optimal compromise between mechanical strength and surface smoothness, while the 5% group showed increased thickness and roughness with slightly lower strength. These findings emphasize that the sol-gel-derived nano-silica from sp. potentially enhances certain characteristics of GIC for possible dental cementation. Further research is needed to determine the long-term durability and bioactivity of these modified materials.