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直接加工和CAD/CAM减材加工树脂复合材料中吸水作用对表面特性和颜色变化的评估

The Evaluation of Water Sorption Effects on Surface Characteristics and Color Changes in Direct and CAD/CAM Subtractively Processed Resin Composites.

作者信息

Osiceanu Georgiana, Bejan Flavia Roxana, Vasiliu Roxana Diana, Porojan Sorin Daniel, Porojan Liliana

机构信息

Department of Dental Prostheses Technology (Dental Technology), Center for Advanced Technologies in Dental Prosthodontics, Faculty of Dental Medicine, "Victor Babes" University of Medicine and Pharmacy Timisoara, Eftimie Murgu Sq. No. 2, 300041 Timisoara, Romania.

Department of Oral Rehabilitation (Dental Technology), Center for Advanced Technologies in Dental Prosthodontics, Faculty of Dental Medicine, "Victor Babes" University of Medicine and Pharmacy Timisoara, Eftimie Murgu Sq. No. 2, 300041 Timisoara, Romania.

出版信息

Materials (Basel). 2025 Apr 15;18(8):1812. doi: 10.3390/ma18081812.

Abstract

This study investigates the influence of water immersion on direct composite resins in comparison with subtractive processed composite resins. It evaluates changes in their optical characteristics, surface roughness, solubility, and water sorption. Four CAD/CAM materials (Vita Enamic, Brilliant, Cerasmart, and Tetric) and three direct composite resins (Gradia Direct Anterior A2, Tetric Evo Ceram A2, and Filtek Z550 A2) were examined. Direct composite samples were created using a 3D-printed mold, compressed, and photopolymerized, whereas CAD/CAM samples were sectioned and processed to the same dimensions. Seventy samples (n = 10) were prepared. After dehydration and initial weighing, samples were immersed in distilled water for 30 days, with mass changes recorded at multiple time points. Surface roughness and optical parameters were measured at three stages: post-dehydration, post-immersion, and post-reconditioning. ANOVA, unpaired and paired Student's -tests, and Pearson correlation coefficient were used to evaluate the variables. The drawn conclusion was that there were significant differences both between stages and between the materials. The most stable material in terms of water sorption was Vita Enamic. Regarding the optical parameters, Brilliant, Vita, and Cerasmart displayed higher stability, while Tetric CAD, Tetric, Gradia, and Filtek showed increased sensitivity to water immersion and re-desiccation. Gradia exhibited the highest surface roughness, while the CAD-CAM materials demonstrated the greatest stability.

摘要

本研究调查了水浸对直接复合树脂的影响,并与减法加工复合树脂进行了比较。它评估了它们在光学特性、表面粗糙度、溶解度和吸水性方面的变化。研究了四种CAD/CAM材料(维他瓷聚体、Brilliant、Cerasmart和Tetric)和三种直接复合树脂(渐变直接前牙A2、Tetric Evo Ceram A2和Filtek Z550 A2)。直接复合树脂样本使用3D打印模具制作、压缩并光固化,而CAD/CAM样本则切割并加工成相同尺寸。制备了70个样本(n = 10)。脱水并初次称重后,将样本浸入蒸馏水中30天,在多个时间点记录质量变化。在三个阶段测量表面粗糙度和光学参数:脱水后、浸泡后和再处理后。使用方差分析、非配对和配对t检验以及皮尔逊相关系数来评估变量。得出的结论是,各阶段之间以及材料之间均存在显著差异。就吸水性而言,最稳定的材料是维他瓷聚体。在光学参数方面,Brilliant、维他和Cerasmart表现出更高的稳定性,而Tetric CAD、Tetric、渐变和Filtek对水浸和再干燥表现出更高的敏感性。渐变表现出最高的表面粗糙度,而CAD/CAM材料表现出最大的稳定性。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b081/12028399/b58e0e1b3d68/materials-18-01812-g001.jpg

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