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从碳源溶剂合成石墨烯的方法学分析。

Methodological analysis of synthesizing graphene from carbon source solvents.

作者信息

Mousanezhad Sedigheh, Bakhshi Hooman

机构信息

Department of Metallurgy Engineering, Sharif University of Technology, Tehran, Iran.

Ro. C., Islamic Azad University, Tehran, Iran.

出版信息

Sci Rep. 2025 Jun 4;15(1):19657. doi: 10.1038/s41598-025-04821-8.

Abstract

This study conducts a methodological analysis of synthesizing graphene from carbon source solvents such as ethanol via self-condensation. The previous methods for fabricating graphene structures from carbon-containing solutions involve intricate multi-step processes that are predicated on specific laboratory configurations, including the utilization of reactors and protective atmospheres, which, due to their complexity, restrict scalability and impede industrial implementation. We have devised a more streamlined methodology by reevaluating the process, which eliminates the necessity for complex laboratory equipment and harsh conditions, thereby facilitating a more practical and scalable route to industrial graphene production. It adheres to green chemistry principles, allowing for the scalable synthesis of graphene oxide (GO) and rGO nanostructures at relatively low temperatures.

摘要

本研究对通过自缩合从乙醇等碳源溶剂合成石墨烯进行了方法学分析。以前从含碳溶液制备石墨烯结构的方法涉及复杂的多步过程,这些过程基于特定的实验室配置,包括使用反应器和保护气氛,由于其复杂性,限制了可扩展性并阻碍了工业应用。我们通过重新评估该过程设计了一种更简化的方法,该方法消除了对复杂实验室设备和苛刻条件的需求,从而为工业石墨烯生产提供了一条更实用、可扩展的途径。它遵循绿色化学原则,能够在相对较低的温度下可扩展地合成氧化石墨烯(GO)和还原氧化石墨烯(rGO)纳米结构。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a182/12137584/7b5b30a8c862/41598_2025_4821_Fig1_HTML.jpg

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