Ashworth R B
J Assoc Off Anal Chem. 1985 Sep-Oct;68(5):1013-8.
A survey of the literature is presented on liquid chromatographic (LC) determination of tetracyclines in plasma, urine, and tissues of food-producing animals. Food Safety and Inspection Service (FSIS) research on tetracyclines during 1973-1984 is discussed, including the thin layer chromatographic qualitative identification method for tissues. Research on development of LC column packings for trace level chromatography of tetracyclines and anhydrotetracyclines is also discussed. Data are shown for recovery, ruggedness testing, and analyst qualification studies on the tentative version of the LC method.
本文介绍了关于液相色谱法(LC)测定食用动物血浆、尿液和组织中四环素的文献综述。讨论了食品安全检验局(FSIS)在1973 - 1984年期间对四环素的研究,包括组织的薄层色谱定性鉴定方法。还讨论了用于四环素和脱水四环素痕量水平色谱分析的液相色谱柱填料的开发研究。展示了关于液相色谱法暂定版本的回收率、耐用性测试和分析人员资质研究的数据。