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牙科树脂复合材料的多模态与高级表征：对饮料诱导降解的见解

Multimodal and Advanced Characterization of Dental Resin Composites: Insights into Beverage-Induced Degradation.

作者信息

Floare Lucian, Dumitrescu Ramona, Bolchis Vanessa, Balean Octavia, Vlase Gabriela, Vlase Titus, Anghel Iasmina-Mădălina, Opris Carmen, Sava-Rosianu Ruxandra, Alexa Vlad Tiberiu, Jumanca Daniela, Galuscan Atena

机构信息

Translational and Experimental Clinical Research Centre in Oral Health, Department of Preventive, Community Dentistry and Oral Health, University of Medicine and Pharmacy "Victor Babes", 300040 Timisoara, Romania.

Clinic of Preventive, Community Dentistry and Oral Health, "Victor Babes" University of Medicine and Pharmacy, Eftimie Murgu Sq. no 2, 300041 Timisoara, Romania.

出版信息

J Clin Med. 2025 Jun 9;14(12):4080. doi: 10.3390/jcm14124080.

DOI:10.3390/jcm14124080
PMID:40565826
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC12199193/
Abstract

: Composite dental restorations are continuously exposed to dietary substances, which may compromise their structural integrity. This study aimed to assess the chemical and mechanical effects of coffee, red wine, and Coca-Cola on two widely used commercial resin composites, Herculite Ultra XRV and Omnichroma. : Forty disk-shaped specimens (20 per material) were immersed for 10 days in the selected beverages. Changes in chemical composition were analyzed using Fourier Transform Infrared (FTIR) and Raman spectroscopy, while Vickers microhardness testing evaluated surface hardness. : FTIR and Raman analyses revealed that coffee and red wine caused the most substantial chemical degradation, particularly in carbonyl (C=O), aromatic (C=C), and siloxane (Si-O-Si) groups. Herculite XRV demonstrated higher chemical stability, while Omnichroma showed more pronounced molecular degradation. In contrast, microhardness testing indicated that Omnichroma maintained better surface hardness compared to Herculite XRV after exposure. Across all solutions, Coca-Cola induced the least effect. : The tested beverages significantly affected both the chemical and mechanical properties of the resin composites. Omnichroma exhibited superior mechanical durability, while Herculite XRV showed greater resistance to chemical degradation. These results highlight the importance of material composition in restorative dentistry and support the development and selection of composites with improved resistance to acidic and staining agents to ensure long-term clinical performance.

摘要

复合牙科修复体持续暴露于饮食物质中，这可能会损害其结构完整性。本研究旨在评估咖啡、红酒和可口可乐对两种广泛使用的商业树脂复合材料Herculite Ultra XRV和Omnichroma的化学和机械影响。40个圆盘形试样（每种材料20个）在选定的饮料中浸泡10天。使用傅里叶变换红外（FTIR）和拉曼光谱分析化学成分的变化，同时通过维氏显微硬度测试评估表面硬度。FTIR和拉曼分析表明，咖啡和红酒造成的化学降解最为显著，尤其是在羰基（C=O）、芳基（C=C）和硅氧烷（Si-O-Si）基团中。Herculite XRV表现出更高的化学稳定性，而Omnichroma的分子降解更为明显。相比之下，显微硬度测试表明，暴露后Omnichroma的表面硬度比Herculite XRV保持得更好。在所有溶液中，可口可乐的影响最小。所测试的饮料对树脂复合材料的化学和机械性能均有显著影响。Omnichroma表现出卓越的机械耐久性，而Herculite XRV对化学降解的抵抗力更强。这些结果突出了材料成分在修复牙科中的重要性，并支持开发和选择对酸性和染色剂具有更高抵抗力的复合材料，以确保长期临床性能。

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本文引用的文献

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J Esthet Restor Dent. 2025 Apr;37(4):1013-1023. doi: 10.1111/jerd.13372. Epub 2024 Nov 30.
2
Microscopic and Color Changes in Direct Dental Restorative Composite Resins upon Immersion in Beverages: Characterization by Scanning Electron Microscopy (SEM) and Energy-Dispersive X-ray Spectroscopy (EDS).直接牙科修复复合树脂浸泡在饮料中的微观和颜色变化：通过扫描电子显微镜（SEM）和能量色散X射线光谱（EDS）进行表征
Biomedicines. 2024 Aug 2;12(8):1740. doi: 10.3390/biomedicines12081740.
3
Enhancing Esthetics in Direct Dental Resin Composite: Investigating Surface Roughness and Color Stability.
提高牙科直接树脂复合材料的美学性能：研究表面粗糙度和颜色稳定性。
J Funct Biomater. 2024 Jul 25;15(8):208. doi: 10.3390/jfb15080208.
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A Historical Perspective on Dental Composite Restorative Materials.牙科复合修复材料的历史视角
J Funct Biomater. 2024 Jun 25;15(7):173. doi: 10.3390/jfb15070173.
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Performance Assessment of Three Similar Dental Restorative Composite Materials via Raman Spectroscopy Supported by Complementary Methods Such as Hardness and Density Measurements.通过拉曼光谱法并辅以硬度和密度测量等补充方法对三种相似牙科修复复合材料进行性能评估
Polymers (Basel). 2024 Feb 7;16(4):466. doi: 10.3390/polym16040466.
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