Sayah Nermine, Ibrahim Nasir A, Elfalleh Walid, Zouari Nacim, Hamdi Noureddine, Jridi Mourad
Laboratory of Functional Physiology and Valorization of Bio-Resources (LR17ES27), Higher Institute of Biotechnology of Beja (ISBB), University of Jendouba, 9000, Beja, Tunisia.
Department of Biology, College of Science, Imam Mohammad Ibn Saud Islamic University (IMSIU), Riyadh 11623, Saudi Arabia.
Food Chem X. 2025 Jun 4;29:102629. doi: 10.1016/j.fochx.2025.102629. eCollection 2025 Jul.
This study investigates the development of biodegradable composite films (F) based on gelatin (G), reinforced with smectite (Sm) and illite (IL) clays as fillers within the biopolymer matrix. A comprehensive set of characterization techniques was employed to evaluate the structural, thermal, mechanical, and barrier properties of the films. Mechanical testing revealed that incorporating 5 % clay significantly enhanced TS while reducing EAB compared to the control. Notably, the gelatin-illite film (GF-IL5%) exhibited superior mechanical stability and lower deformability compared to the gelatin-smectite counterpart (GF-Sm5%). Contact angle measurements indicated increased surface hydrophobicity, consistent with reduced WVP, suggesting improved barrier functionality. Additionally, the films showed enhanced antibacterial and antioxidant activities. Biodegradability tests and preservation trials on cherry fruits demonstrated that GF-Sm5% and GF-IL5% films contribute to prolong fruit freshness and microbial stability. These findings highlight the potential of Sm- and IL-reinforced gelatin films as high-performance materials for food preservation applications.
本研究调查了以明胶(G)为基础、用蒙脱石(Sm)和伊利石(IL)粘土作为填料在生物聚合物基质中增强的可生物降解复合薄膜(F)的开发情况。采用了一套全面的表征技术来评估薄膜的结构、热性能、机械性能和阻隔性能。机械测试表明,与对照相比,加入5%的粘土显著提高了拉伸强度(TS),同时降低了断裂伸长率(EAB)。值得注意的是,与明胶-蒙脱石薄膜(GF-Sm5%)相比,明胶-伊利石薄膜(GF-IL5%)表现出更高的机械稳定性和更低的变形性。接触角测量表明表面疏水性增加,这与水蒸气透过率(WVP)降低一致,表明阻隔功能得到改善。此外,这些薄膜还表现出增强的抗菌和抗氧化活性。对樱桃果实的生物降解性测试和保鲜试验表明,GF-Sm5%和GF-IL5%薄膜有助于延长果实的新鲜度和微生物稳定性。这些发现突出了蒙脱石和伊利石增强的明胶薄膜作为食品保鲜应用高性能材料的潜力。