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不同黏合剂和表面处理对修复型大块充填复合材料的剪切和拉伸黏结强度及微渗漏的影响,并通过微型计算机断层扫描进行研究

Influence of Different Adhesives and Surface Treatments on Shear and Tensile Bond Strength and Microleakage with Micro-CT of Repaired Bulk-Fill Composites.

作者信息

Yıldırım-Işık Handan, Büyükgöze-Dindar Mediha

机构信息

Department of Restorative Dentistry, Faculty of Dentistry, Istanbul Beykent University, 34500 Istanbul, Turkey.

Heath Services Vocational School, Trakya University, 22030 Edirne, Turkey.

出版信息

Polymers (Basel). 2025 Jun 17;17(12):1680. doi: 10.3390/polym17121680.

DOI:10.3390/polym17121680
PMID:40574209
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC12196890/
Abstract

The repair of defective composite restorations, particularly bulk-fill composites, offers a conservative alternative to complete replacement. However, establishing durable adhesion between aged and fresh composites remains a clinical challenge due to the altered surface properties of aged materials. This in vitro study investigated the effects of different surface treatment protocols (no treatment, diamond bur roughening, and air abrasion) and adhesive systems (G-Premio Bond, Clearfil SE Bond, and Adper Single Bond 2) on the shear bond strength (µSBS), tensile bond strength (µTBS), and microleakage of repaired bulk-fill composites. Results demonstrated that both surface treatment and adhesive type significantly affected bond strength ( < 0.05). Mechanical surface treatments, particularly diamond bur roughening and air abrasion, enhanced µSBS and µTBS compared to untreated controls. The highest µSBS and µTBS values were observed with diamond bur treatment combined with Adper Single Bond 2, reaching mean values of 25.8 ± 2.1 MPa and 28.3 ± 1.8 MPa, respectively. Air abrasion with Clearfil SE Bond also significantly increased bond strengths (µSBS: 22.1 ± 2.0 MPa; µTBS: 23.5 ± 1.7 MPa) relative to no treatment ( < 0.05). Micro-computed tomography analysis revealed that Clearfil SE Bond following diamond bur roughening resulted in the lowest microleakage scores, with a mean leakage volume of 0.12 ± 0.04 µm. These findings underscore the importance of mechanical surface conditioning and appropriate adhesive selection to enhance both bond strength and sealing efficacy in composite repair procedures.

摘要

修复有缺陷的复合树脂修复体,尤其是大块充填复合树脂,为完全替换提供了一种保守的替代方法。然而,由于老化材料表面性质的改变,在老化和新鲜复合树脂之间建立持久的粘结力仍然是一个临床挑战。这项体外研究调查了不同表面处理方案(不处理、金刚砂车针粗化和空气喷砂)和粘结系统(G-Premio Bond、Clearfil SE Bond和Adper Single Bond 2)对修复的大块充填复合树脂的剪切粘结强度(µSBS)、拉伸粘结强度(µTBS)和微渗漏的影响。结果表明,表面处理和粘结剂类型均对粘结强度有显著影响(<0.05)。与未处理的对照组相比,机械表面处理,尤其是金刚砂车针粗化和空气喷砂,提高了µSBS和µTBS。使用金刚砂车针处理结合Adper Single Bond 2观察到最高的µSBS和µTBS值,分别达到平均值25.8±2.1MPa和28.3±1.8MPa。相对于未处理,使用Clearfil SE Bond进行空气喷砂也显著提高了粘结强度(µSBS:22.1±2.0MPa;µTBS:23.5±1.7MPa)(<0.05)。微计算机断层扫描分析显示,金刚砂车针粗化后使用Clearfil SE Bond导致微渗漏评分最低,平均渗漏体积为0.12±0.04µm。这些发现强调了机械表面预处理和选择合适的粘结剂对于提高复合树脂修复程序中的粘结强度和密封效果的重要性。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e931/12196890/6415b13f2a34/polymers-17-01680-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e931/12196890/134212b83705/polymers-17-01680-g001.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e931/12196890/3a49412ea5e0/polymers-17-01680-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e931/12196890/84f126b26217/polymers-17-01680-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e931/12196890/91559103d1ac/polymers-17-01680-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e931/12196890/15a07659260b/polymers-17-01680-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e931/12196890/fed586f94159/polymers-17-01680-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e931/12196890/6415b13f2a34/polymers-17-01680-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e931/12196890/134212b83705/polymers-17-01680-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e931/12196890/83c4d1b54dae/polymers-17-01680-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e931/12196890/3a49412ea5e0/polymers-17-01680-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e931/12196890/84f126b26217/polymers-17-01680-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e931/12196890/91559103d1ac/polymers-17-01680-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e931/12196890/15a07659260b/polymers-17-01680-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e931/12196890/fed586f94159/polymers-17-01680-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e931/12196890/6415b13f2a34/polymers-17-01680-g008.jpg

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