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巴西红蜂胶对甲基丙烯酸酯类粘结剂微拉伸粘结强度和封闭能力的影响。

Effect of Brazilian red propolis on microtensile bond strength and sealing ability of the methacrylate-based bonding agents.

作者信息

Vidal Gustavo César Feitosa, Balbino Edson Philippe Bezerra, Oliveira José Marcos Dos Santos, Dos Santos Natanael Barbosa, Lôbo Teresa de Lisieux Guedes Ferreira, do Nascimento Ticiano Gomes, de Freitas Johnnatan Duarte, de Freitas Jeniffer Mclaine Duarte, Porto Isabel Cristina Celerino de Moraes

机构信息

Federal University of Alagoas, Faculty of Dentistry.

Federal University of Alagoas, Institute of Pharmaceutical Sciences.

出版信息

J Clin Exp Dent. 2025 Jun 1;17(6):e665-e674. doi: 10.4317/jced.62587. eCollection 2025 Jun.

Abstract

BACKGROUND

The aim of the study was to analyze the sealing ability and microtensile bond strength of a dental adhesive with propolis.

MATERIAL AND METHODS

Red propolis extract was added to an experimental methacrylate-based adhesive (EA) at following concentrations: 100 (EA PV100), 250 (EA PV250) e 500 μg/mL (EA PV500). Single Bond Universal adhesive (SB) and EA without propolis were used as controls. The effectiveness of the dentin sealing was evaluated at nanoscale (silver uptake) and microscale (dye microleakage). Microtensile bond strength (µTBS) was measured 24 hours after the bonding process. Data were analyzed by one-way ANOVA and Tukey's test (α=0.05).

RESULTS

EA PV500 showed the best coronal sealing, with better performance than the control and the commercial adhesive. Immediate µTBS values ranged from 28.94 + 9.25 MPa (EA PV100) to 39.09 + 9.60 MPa (SB). Comparing SB and EA with propolis, a significant decrease in µTBS was noted (<0.05). The EA without propolis had similar performance to SB (=1.000).

CONCLUSIONS

Nanoleakage and microleakage were not eliminated in any of the groups, but EA PV500 µg/mL exhibited the best sealing ability, with superior performance compared to the control and commercial adhesive. A decrease in μTBS of AE with propolis was observed. Dentin-bonding agents, Propolis, Dental materials, Dental marginal adaptation.

摘要

背景

本研究的目的是分析含蜂胶的牙科粘合剂的封闭能力和微拉伸粘结强度。

材料与方法

将红色蜂胶提取物以以下浓度添加到基于甲基丙烯酸酯的实验性粘合剂(EA)中:100(EA PV100)、250(EA PV250)和500μg/mL(EA PV500)。使用单键通用粘合剂(SB)和不含蜂胶的EA作为对照。在纳米尺度(银摄取)和微观尺度(染料微渗漏)上评估牙本质封闭的有效性。在粘结过程24小时后测量微拉伸粘结强度(µTBS)。数据通过单因素方差分析和Tukey检验进行分析(α=0.05)。

结果

EA PV500表现出最佳的冠部封闭效果,性能优于对照和市售粘合剂。即时µTBS值范围为28.94 + 9.25MPa(EA PV100)至39.09 + 9.60MPa(SB)。与含蜂胶的SB和EA相比,µTBS显著降低(<0.05)。不含蜂胶的EA与SB性能相似(=1.000)。

结论

所有组均未消除纳米渗漏和微渗漏,但EA PV500µg/mL表现出最佳的封闭能力,与对照和市售粘合剂相比性能更优。观察到含蜂胶的AE的µTBS有所降低。牙本质粘结剂、蜂胶、牙科材料、牙边缘适应性。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/616c/12225770/ffae3eecc656/jced-17-06-e665-g001.jpg

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