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不同老化模式对不同氧化钇浓度的氧化锆在咖啡和茶中的光学性能的影响。

Effects of various aging modes on the optical properties of zirconia with different yttria concentrations in coffee and tea.

作者信息

Tseng Chih-Wei, Yao Chenmin, Wei Liang-Yu, Peng Pei-Wen, Lin Wei-Chun

机构信息

Department of Dentistry, Wan Fang Hospital, Taipei Medical University, Taipei, Taiwan.

School of Dentistry, College of Oral Medicine, Taipei Medical University, Taipei, Taiwan.

出版信息

J Dent Sci. 2025 Jul;20(3):1764-1771. doi: 10.1016/j.jds.2025.04.017. Epub 2025 Apr 22.

Abstract

BACKGROUND/PURPOSE: The esthetic performance of dental zirconia may be affected by both material composition and environmental exposure. This study aimed to evaluate how different aging conditions-hydrothermal aging and thermal cycling-influenced the optical properties of dental zirconia containing varying yttria concentrations (3Y-TZP, 4Y-TZP, and 5Y-TZP) in coffee and tea.

MATERIALS AND METHODS

A total of 120 zirconia specimens were prepared using three yttria concentrations. Each group was subjected to four artificial aging conditions: storage in coffee or tea at 37 °C for 1 and 6 months (hydrothermal aging), or 10,000 and 50,000 cycles of thermal cycling between 5 °C and 55 °C. Optical parameters (L∗, a∗, b∗) and color differences (ΔE) were measured using a spectrophotometer and calculated using the CIEDE2000 formula. Data were analyzed using ANOVA and Tukey's HSD test (α = 0.05).

RESULTS

Zirconia with higher yttria content exhibited more pronounced color changes ( < 0.001). Aging in tea resulted in minimal color variation regardless of yttria content or aging mode. In coffee, the ΔE values of the HT (3Y-TZP), ST (4Y-TZP), and XT (5Y-TZP) groups ranged from 3.5, 7.0 and 8.5, respectively ( < 0.0001). In tea, the values ranged from 1.1 for both HT and ST, and from 3.1 for XT ( < 0.0001).

CONCLUSION

Both yttria concentration and aging conditions significantly influenced the color stability of zirconia. Hydrothermal aging had a greater impact than thermal cycling, especially in coffee. These findings suggest that material composition and exposure environment should be carefully considered when selecting zirconia for esthetic dental restorations.

摘要

背景/目的:牙科氧化锆的美学性能可能会受到材料成分和环境暴露的影响。本研究旨在评估不同的老化条件——水热老化和热循环——如何影响含不同氧化钇浓度(3Y-TZP、4Y-TZP和5Y-TZP)的牙科氧化锆在咖啡和茶中的光学性能。

材料与方法

使用三种氧化钇浓度制备了总共120个氧化锆试样。每组分别经受四种人工老化条件:在37℃的咖啡或茶中储存1个月和6个月(水热老化),或在5℃至55℃之间进行10000次和50000次热循环。使用分光光度计测量光学参数(L∗、a∗、b∗)并使用CIEDE2000公式计算颜色差异(ΔE)。数据采用方差分析和Tukey's HSD检验进行分析(α = 0.05)。

结果

氧化钇含量较高的氧化锆表现出更明显的颜色变化(<0.001)。无论氧化钇含量或老化方式如何,在茶中老化导致的颜色变化最小。在咖啡中,HT(3Y-TZP)、ST(4Y-TZP)和XT(5Y-TZP)组的ΔE值分别为3.5、7.0和8.5(<0.0001)。在茶中,HT和ST组的值均为1.1,XT组为3.1(<0.0001)。

结论

氧化钇浓度和老化条件均显著影响氧化锆的颜色稳定性。水热老化比热循环的影响更大,尤其是在咖啡中。这些发现表明,在选择用于美学牙科修复的氧化锆时,应仔细考虑材料成分和暴露环境。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/98bd/12254836/b1ca6ec710ae/gr1.jpg

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