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两种从花生粕和花生酱中提取黄曲霉毒素方法的比较研究。

Comparative study of two methods for extraction of aflatoxin from peanut meal and peanut butter.

作者信息

Chang H H, De Vries J W, Hobbs W E

出版信息

J Assoc Off Anal Chem. 1979 Nov;62(6):1281-4.

PMID:521413
Abstract

The difference between the CB and Best Foods methods in extracting aflatoxins from peanut products has been studied. The CB method yields 60, 121, 35, and 22% higher results for aflatoxins B1, B2, G1, and G2, respectively for 4 samples of peanut meal and 6 samples of peanut butter studied. Both reverse phase liquid chromatography and thin layer chromatography were used to quantitate the extracted aflatoxins.

摘要

已对CB法和最佳食品法从花生制品中提取黄曲霉毒素的差异进行了研究。对于所研究的4份花生粕样品和6份花生酱样品,CB法对黄曲霉毒素B1、B2、G1和G2的提取结果分别高出60%、121%、35%和22%。采用反相液相色谱法和薄层色谱法对提取的黄曲霉毒素进行定量。

相似文献

1
Comparative study of two methods for extraction of aflatoxin from peanut meal and peanut butter.两种从花生粕和花生酱中提取黄曲霉毒素方法的比较研究。
J Assoc Off Anal Chem. 1979 Nov;62(6):1281-4.
2
Determination of aflatoxins in peanut butter, using two liquid chromatographic methods: collaborative study.采用两种液相色谱法测定花生酱中的黄曲霉毒素:协同研究
J Assoc Off Anal Chem. 1984 Mar-Apr;67(2):312-6.
3
Improved liquid chromatographic method for determination of aflatoxins in peanut butter and other commodities.用于测定花生酱及其他商品中黄曲霉毒素的改进液相色谱法。
J Assoc Off Anal Chem. 1984 May-Jun;67(3):597-600.
4
Reverse phase high pressure liquid chromatographic determination of aflatoxins in foods.反相高效液相色谱法测定食品中的黄曲霉毒素
J Assoc Off Anal Chem. 1978 Nov;61(6):1347-52.
5
High pressure liquid chromatographic determination of aflatoxins in peanut butter using a silica gel-packed flowcell for fluorescence detection.使用硅胶填充流通池进行荧光检测的高效液相色谱法测定花生酱中的黄曲霉毒素
J Assoc Off Anal Chem. 1982 May;65(3):672-6.
6
Comparison of rapid high pressure liquid chromatographic and CB methods for determination of aflatoxins in corn and peanuts.快速高压液相色谱法与CB法测定玉米和花生中黄曲霉毒素的比较
J Assoc Off Anal Chem. 1982 Mar;65(2):206-9.
7
International mycotoxin check sample program. Part I. Report on the performance of participating laboratories.国际霉菌毒素检测样品计划。第一部分。参与实验室的性能报告。
J Assoc Off Anal Chem. 1980 Sep;63(5):1057-66.
8
Evaluation of enzyme-linked immunosorbent assay of cleanup for thin-layer chromatography of aflatoxin B1 in corn, peanuts, and peanut butter.玉米、花生和花生酱中黄曲霉毒素B1薄层色谱法净化的酶联免疫吸附测定评估。
J Assoc Off Anal Chem. 1988 Sep-Oct;71(5):953-6.
9
Comparison of liquid chromatography and high performance thin layer chromatography for determination of aflatoxin in peanut products.液相色谱法与高效薄层色谱法测定花生制品中黄曲霉毒素的比较。
J Assoc Off Anal Chem. 1984 Mar-Apr;67(2):337-9.
10
Rapid determination of aflatoxins in raw peanuts by liquid chromatography with postcolumn iodination and modified minicolumn cleanup.采用柱后碘化和改良微柱净化的液相色谱法快速测定生花生中的黄曲霉毒素。
J Assoc Off Anal Chem. 1988 Jan-Feb;71(1):43-7.

引用本文的文献

1
Analytical methods for the determination of aflatoxins in various food matrices at concentrations regarding the limits set in european regulations: development, characteristics, limits.各种食品基质中黄曲霉毒素浓度的分析方法:发展、特点、限量。
Mycotoxin Res. 2000 Mar;16(1):23-42. doi: 10.1007/BF02946103.
2
Evaluation of silica cartridge purification and hemiacetal formation for liquid chromatographic determination of aflatoxins in corn.用于液相色谱法测定玉米中黄曲霉毒素的硅胶柱净化及半缩醛形成的评估
Arch Environ Contam Toxicol. 1989 May-Jun;18(3):319-26. doi: 10.1007/BF01062355.