Tsvetkova Ts, Grigorova D
Vet Med Nauki. 1979;16(6):16-20.
A modification of the method for determining benzoic acid and its salts by water-vapour distillation and extraction of the biological material conservant and its titrimetrical determination is proposed. The thin layer chromatography method (TLC) is used parallelly for the identification of the conservant. The advantage of the proposed method consists in that the same distiller is used for quantitative titrimetrical determination and for TLC assessment. The method possesses high sensitivity 1 gamma in TLC scoring and 0.1 mg in titrimetric determination. It is applied for the determination of conservants in various fish assortments, canned fish and roe.
提出了一种改进的方法,用于通过水蒸气蒸馏和提取生物材料防腐剂来测定苯甲酸及其盐类,并进行滴定测定。同时采用薄层色谱法(TLC)对防腐剂进行鉴定。所提方法的优点在于,同一蒸馏器用于定量滴定测定和TLC评估。该方法具有高灵敏度,TLC评分可达1微克,滴定测定可达0.1毫克。它适用于测定各种鱼类、罐装鱼和鱼籽中的防腐剂。