Miles P
J Assoc Off Anal Chem. 1978 Nov;61(6):1366-9.
An ion selective electrode procedure is described for the precise, accurate determination of iodide at the sub-ppm level in a variety of nutritional beverages. The relative standard deviation of the analysis is 1--4%; recoveries range from 90 to 120%. Comparison with results from neutron activation analysis and the traditional Sandell-Kolthoff procedure shows that the ion selective electrode procedure is free of determine error and that dry ashing of samples can lead to low results.
描述了一种离子选择性电极法,用于精确、准确地测定各种营养饮料中亚ppm水平的碘化物。分析的相对标准偏差为1%-4%;回收率在90%至120%之间。与中子活化分析结果和传统的桑德尔-科尔托夫法比较表明,离子选择性电极法无测定误差,样品干灰化会导致结果偏低。