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[使用Silufol成品板上的薄层色谱法对山梨糖和山梨醇进行纯度测试]

[Purity testing of sorbose and sorbitol using thin layer chromatography on Silufol finished plates].

作者信息

Illner E

出版信息

Pharmazie. 1984 Oct;39(10):689-90.

PMID:6441171
Abstract

Different methods had been elaborated for proof and semiquantitative determination of mono-, di- and trisaccharides and of mannitol and sorbitol in sorbose as well as of mannitol, mono-, di- and trisaccharides in sorbitol following their separation by means of Silufol finished plates UV254. According to the results of sample mixtures, there is the possibility to separate from sorbose and to semiquantitatively determine 0.5% fructose and glucose each, 0.3 to 0.5% di- and trisaccharides as well as 1% sorbitol and 5% mannitol. Furthermore 0.5% fructose and glucose each, 0.3-0.5% di- and trisaccharides as well as 5% mannitol can be separated from sorbitol and semiquantitatively be determined.

摘要

已制定了不同方法,用于在山梨糖中对单糖、二糖和三糖以及甘露醇和山梨醇进行定性和半定量测定,以及在山梨醇经Silufol成品板UV254分离后对甘露醇、单糖、二糖和三糖进行测定。根据样品混合物的结果,有可能从山梨糖中分离出并半定量测定各0.5%的果糖和葡萄糖、0.3%至0.5%的二糖和三糖以及1%的山梨醇和5%的甘露醇。此外,各0.5%的果糖和葡萄糖、0.3 - 0.5%的二糖和三糖以及5%的甘露醇可从山梨醇中分离出来并进行半定量测定。

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