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采用液相色谱-安培检测法测定生物基质中的草酸。

Determination of oxalic acid in biological matrices by liquid chromatography with amperometric detection.

作者信息

Kok W T, Groenendijk G, Brinkman U A, Frei R W

出版信息

J Chromatogr. 1984 Dec 19;315:271-8. doi: 10.1016/s0021-9673(01)90744-7.

DOI:10.1016/s0021-9673(01)90744-7
PMID:6526899
Abstract

Oxalic acid was separated from interfering compounds with a solvent-generated ion-exchange chromatographic system, and detected with a copper electrode amperometric detector. The lower limit of detection in standard solutions was 5 ng. Complex samples, such as vegetable extracts and urine, could be analysed with a minimum of sample preparation.

摘要

采用溶剂生成离子交换色谱系统将草酸与干扰化合物分离,并用铜电极安培检测器进行检测。标准溶液中的检测下限为5纳克。对于复杂样品,如蔬菜提取物和尿液,只需进行最少的样品制备即可进行分析。

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