Sood S, Firnau G, Garnett E S
Int J Appl Radiat Isot. 1983 Apr;34(4):743-5. doi: 10.1016/0020-708x(83)90254-5.
The reaction between [18F]xenon difluoride, 3,4,6-tri-O-acetyl-D-glucal and boron trifluoride in ether gives exclusively [18F )3,4,6-tri-O-acetyl-2-fluoro-2-deoxy-D-glucopyranosyl fluoride, which is hydrolysed with 1 N HCl to [18F]2-fluoro-2-deoxy-D-glucose. The overall chemical yield is 75%; the radiochemical yield is 20%. The procedure takes 45 min.
[18F]二氟化氙、3,4,6-三-O-乙酰基-D-葡糖醛与三氟化硼在乙醚中的反应仅生成[18F]3,4,6-三-O-乙酰基-2-氟-2-脱氧-D-吡喃葡萄糖基氟化物，该化合物用1N盐酸水解生成[18F]2-氟-2-脱氧-D-葡萄糖。总化学产率为75%；放射化学产率为20%。该过程耗时45分钟。
Zotero 插件