一种用于定量脑组织和尿液中2-苯乙胺的快速灵敏气相色谱法。
A rapid and sensitive gas chromatographic method for quantitation of 2-phenylethylamine in brain tissue and urine.
作者信息
Hampson D R, Baker G B, Coutts R T
出版信息
Res Commun Chem Pathol Pharmacol. 1984 Jan;43(1):169-72.
PMID:6701400
Abstract
A rapid, sensitive procedure for analysis of 2-phenylethylamine in brain tissue and urine is described. The method involves extraction with a liquid ion exchanger, elution with HCl, acetylation under aqueous conditions, pentafluorobenzoylation under anhydrous conditions and analysis using a gas chromatograph equipped with a capillary column and an electron-capture detector.
摘要
本文描述了一种快速、灵敏的分析脑组织和尿液中2-苯乙胺的方法。该方法包括用液体离子交换剂萃取、用盐酸洗脱、在水相条件下乙酰化、在无水条件下五氟苯甲酰化以及使用配备毛细管柱和电子捕获检测器的气相色谱仪进行分析。
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