一种用于定量脑组织和尿液中2-苯乙胺的快速灵敏气相色谱法。
A rapid and sensitive gas chromatographic method for quantitation of 2-phenylethylamine in brain tissue and urine.
作者信息
Hampson D R, Baker G B, Coutts R T
出版信息
Res Commun Chem Pathol Pharmacol. 1984 Jan;43(1):169-72.
PMID:6701400
Abstract
A rapid, sensitive procedure for analysis of 2-phenylethylamine in brain tissue and urine is described. The method involves extraction with a liquid ion exchanger, elution with HCl, acetylation under aqueous conditions, pentafluorobenzoylation under anhydrous conditions and analysis using a gas chromatograph equipped with a capillary column and an electron-capture detector.
摘要
本文描述了一种快速、灵敏的分析脑组织和尿液中2-苯乙胺的方法。该方法包括用液体离子交换剂萃取、用盐酸洗脱、在水相条件下乙酰化、在无水条件下五氟苯甲酰化以及使用配备毛细管柱和电子捕获检测器的气相色谱仪进行分析。
相似文献
1
A rapid and sensitive gas chromatographic method for quantitation of 2-phenylethylamine in brain tissue and urine.
Res Commun Chem Pathol Pharmacol. 1984 Jan;43(1):169-72.
2
A rapid, sensitive assay for gamma-aminobutyric acid in brain using electron-capture gas chromatography.
Res Commun Chem Pathol Pharmacol. 1990 Oct;70(1):115-24.
3
An electron-capture gas chromatographic method for analysis of urinary 3-methoxy-4-hydroxyphenylethylene glycol (MHPG).
Res Commun Chem Pathol Pharmacol. 1986 Oct;54(1):141-4.
4
Rapid analysis of beta-phenylethylamine in tissues and body fluids utilizing pentafluorobenzoylation followed by electron-capture gas chromatography.
Prog Neuropsychopharmacol Biol Psychiatry. 1987;11(2-3):251-8. doi: 10.1016/0278-5846(87)90068-6.
5
Electron-capture gas chromatographic analysis of beta-phenylethylamine in tissues and body fluids using pentafluorobenzenesulfonyl chloride for derivatization.
J Chromatogr. 1986 Sep 5;381(2):211-7. doi: 10.1016/s0378-4347(00)83586-0.
6
A rapid and sensitive procedure for the simultaneous analysis of beta-phenylethylamine and tranylcypromine in rat brain using trichloroacetylation and gas chromatography.
Res Commun Chem Pathol Pharmacol. 1985 Sep;49(3):471-4.
7
Determination of beta-phenylethylamine as its isothiocyanate derivative in biological samples by gas chromatography mass spectrometry.
Biomed Mass Spectrom. 1983 Jul;10(7):430-3. doi: 10.1002/bms.1200100708.
8
Rapid and sensitive determination of beta-phenylethylamine in animal brains by high performance liquid chromatography with fluorometric detection.
Biomed Chromatogr. 1989 May;3(3):118-20. doi: 10.1002/bmc.1130030306.
9
Procedural difficulties in the gas-liquid chromatographic assay of the arylalkylamines.
J Chromatogr. 1976 Jul 21;123(1):45-50. doi: 10.1016/s0021-9673(00)81100-0.
10
Analysis of the antidepressant phenelzine in brain tissue and urine using electron-capture gas chromatography.
J Pharmacol Methods. 1987 Jul;17(4):297-304. doi: 10.1016/0160-5402(87)90043-x.
Zotero 插件