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静脉注射液中特布他林、儿茶酚胺与氨茶碱的离子对高效液相色谱法

Ion-pair high-performance liquid chromatography of terbutaline and catecholamines with aminophylline in intravenous solutions.

作者信息

Williams D A, Fung E Y, Newton D W

出版信息

J Pharm Sci. 1982 Aug;71(8):956-8. doi: 10.1002/jps.2600710832.

DOI:10.1002/jps.2600710832
PMID:7120108
Abstract

A stability-indicating ion-pair high-performance liquid chromatographic (HPLC) assay that is rapid and specific for epinephrine, isoproterenol, dopamine, norepinephrine, methyldopate, or terbutaline in intravenous solutions with aminophylline has been developed using a spectrofluorometric detector. A HPLC method for the analysis of terbutaline and methyldopate is introduced, and the superiority of fluorometric over UV detection of terbutaline and the catecholamines is illustrated.

摘要

已开发出一种稳定性指示离子对高效液相色谱（HPLC）分析法，该方法使用荧光分光检测器，可快速、特异性地测定静脉用氨茶碱溶液中的肾上腺素、异丙肾上腺素、多巴胺、去甲肾上腺素、甲基多巴酯或特布他林。本文介绍了一种分析特布他林和甲基多巴酯的HPLC方法，并说明了荧光检测相对于紫外检测特布他林和儿茶酚胺的优越性。

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