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改进开发以提高用于能量更高的同位素的AR10剥离乳液的性能。

Modified development to improve the performance of AR10 stripping emulsions for use with the more energetic isotopes.

作者信息

Sanderson J

出版信息

J Microsc. 1981 Nov;124(Pt 2):177-82. doi: 10.1111/j.1365-2818.1981.tb00311.x.

Abstract

Gold latensification of the image to increase the efficiency of the more energetic isotopes, such as 14 carbon, has been used before for liquid emulsions, with mild developers, but never successfully with AR10 stripping emulsion. This paper describes the performance of different developers and assesses their ability to suppress background fog on Kodak AR10 emulsion. A 14 carbon source was used and the effect of gold latensification was examined. Kodak D19, an efficient Metol/hydroquinone developer, could be usefully modified by altering the sodium carbonate and sulphite contents (D19 A/S). This developer discriminated well against the background with AR10 emulsion, producing a far better signal:background ratio than Kodak D19. A pretreatment in aurous thiocyanate for 4 min before development in D19 A/S for 4 min at 291 K increased the signal:background ratio by 200% compared with ordinary development in Kodak D19. When gold latensification was used with D19 developer, the signal was increased, but not more than with D19 A/S, and the gain was offset by the intense background that resulted.

摘要

为提高诸如碳 - 14等能量较高的同位素成像效率而进行的金增感,此前已用于液体乳剂,使用的是温和显影剂,但在AR10剥离乳剂中从未成功过。本文描述了不同显影剂的性能,并评估了它们抑制柯达AR10乳剂背景灰雾的能力。使用了碳 - 14源,并研究了金增感的效果。柯达D19是一种高效的米吐尔/对苯二酚显影剂,可以通过改变碳酸钠和亚硫酸盐含量(D19 A/S)进行有效改性。这种显影剂在AR10乳剂中对背景的区分效果很好,产生的信号与背景比远优于柯达D19。在291K下,先在硫氰酸金中预处理4分钟,然后在D19 A/S中显影4分钟,与在柯达D19中常规显影相比,信号与背景比提高了200%。当金增感与D19显影剂一起使用时,信号增加了,但不超过D19 A/S,并且增益被由此产生的强烈背景抵消。

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