Yang J, Liu W, Chen Y, Zhong X, Qin Y
Guiyang College of Traditional Chinese Medicine.
Zhongguo Zhong Yao Za Zhi. 1995 Jun;20(6):346-8, 383.
The extraction and purificatory crafts for Radix Sophorae Flavescentis were observed through the orthogonal experiment design using matrine as the fixed indicatrix for TLC-scanning. Quantitative analyses of matrine were made on the momentum parameters of the different craft conditions. The results of the three different extraction methods show that the best way is to use 2% gelatin to remove tannin with the least loss of matrine, and that the ethanol extract from water precitation is better than the water extract from ethanol precipitation.
以苦参碱为TLC扫描固定指标,采用正交试验设计观察苦参的提取与纯化工艺。对不同工艺条件下的动量参数进行苦参碱的定量分析。三种不同提取方法的结果表明,最佳方法是用2%明胶去除鞣质,苦参碱损失最少,且水沉乙醇提取物优于醇沉水提取物。