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加工后软质义齿衬垫的动态粘弹性特性:第一部分——初始特性。

Dynamic viscoelastic properties of processed soft denture liners: Part I--Initial properties.

作者信息

Wagner W C, Kawano F, Dootz E R, Koran A

机构信息

Biologic and Materials Sciences Department, School of Dentistry, University of Michigan, Ann Arbor, USA.

出版信息

J Prosthet Dent. 1995 May;73(5):471-7. doi: 10.1016/s0022-3913(05)80077-0.

Abstract

This research evaluated the dynamic viscoelastic properties of 12 laboratory-processed soft denture liners. Specimens, 1.4 x 3 x 40 mm, were prepared according to the manufacturer's instructions. Five specimens of each material were tested under applied strain frequencies of 1, 5, or 10 Hz and temperatures of 23 degrees C and 37 degrees C. The values at 37 degrees C and 1 Hz were judged most important because they closely approximate the service environment; therefore material comparisons were made for these conditions. Samples were tested with a custom-made dynamic viscoelastometer. The statistical significance of the results was tested by ANOVA and Scheffe's intervals test. Large differences in the storage modulus (elastic stiffness) were found. One acrylic resin, Verno-Soft, showed significantly higher storage moduli than the other materials. The viscous behavior of the materials was reflected by the loss modulus; here large differences were also found. Verno-Soft again exhibited much higher values than all of the other materials. Three other acrylic resins (Super Soft, Soft-Pak, and Justi Soft) also showed significantly higher loss moduli than the other materials. Significant differences were found in the damping factor between many of the materials. Most of the acrylic and vinyl resins had higher damping factors than the silicone and polyphosphazine rubbers. The values of the storage moduli, loss moduli, and the damping factor were affected by temperature and by applied strain frequency with some materials.

摘要

本研究评估了12种实验室加工的软质义齿衬垫材料的动态粘弹性。按照制造商的说明制备尺寸为1.4×3×40毫米的试样。每种材料取5个试样,在1、5或10赫兹的施加应变频率以及23℃和37℃的温度下进行测试。37℃和1赫兹时的值被认为最为重要,因为它们非常接近使用环境;因此在这些条件下进行了材料比较。使用定制的动态粘弹性仪对样品进行测试。结果的统计学显著性通过方差分析和谢费区间检验进行测试。发现储能模量(弹性刚度)存在很大差异。一种丙烯酸树脂Verno-Soft的储能模量显著高于其他材料。损耗模量反映了材料的粘性行为;此处也发现了很大差异。Verno-Soft的损耗模量再次远高于所有其他材料。另外三种丙烯酸树脂(Super Soft、Soft-Pak和Justi Soft)的损耗模量也显著高于其他材料。许多材料之间的阻尼因子存在显著差异。大多数丙烯酸树脂和乙烯基树脂的阻尼因子高于硅树脂和聚磷腈橡胶。储能模量、损耗模量和阻尼因子的值受温度和一些材料的施加应变频率的影响。

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