Murat H, Taguchi N, Hamada T, McCabe J F
Department of Prosthetic Dentistry, Hiroshima University Faculty of Dentistry, Japan.
Biomaterials. 2000 Jul;21(14):1421-7. doi: 10.1016/s0142-9612(00)00010-7.
The dynamic viscoelastic properties of long-term soft denture liners were measured over a wide range of frequencies using a dynamic viscoelastometer based on a non-resonance-forced vibration principle. Changes in properties over a 3 yr period have also been monitored. One acrylic material, one fluoroelastomer, one heat cured silicone and one self-curing addition silicone were used. Complex dynamic tensile modulus (E*), tensile storage modulus (E'), tensile loss modulus (E") and loss tangent (tan delta) were determined over the frequency range from 0.01 to 100 Hz on administration of a 0.27% strain at 37 degrees C. The dynamic viscoelasticity of the acrylic and fluoroelastomer products was more sensitive to changes in frequency than that of silicone products. The acrylic material and fluoroelastomer exhibited viscoelastic behaviour whilst silicones exhibited elastic behaviour. The silicone products remained unchanged after soaking for 3 yr whilst the acrylic and fluoroelastomer products underwent significant change.
使用基于非共振强迫振动原理的动态粘弹性仪,在很宽的频率范围内测量了长期使用的软质义齿衬垫材料的动态粘弹性特性。还监测了这些材料在3年期间的性能变化。使用了一种丙烯酸材料、一种氟弹性体、一种热固化硅橡胶和一种自固化加成型硅橡胶。在37℃施加0.27%应变的情况下,在0.01至100Hz的频率范围内测定了复数动态拉伸模量(E*)、拉伸储能模量(E')、拉伸损耗模量(E")和损耗角正切(tanδ)。丙烯酸材料和氟弹性体产品的动态粘弹性比硅橡胶产品对频率变化更敏感。丙烯酸材料和氟弹性体表现出粘弹性行为,而硅橡胶表现出弹性行为。硅橡胶产品浸泡3年后没有变化,而丙烯酸材料和氟弹性体产品发生了显著变化。