小分子和肽在大孔聚（苯乙烯 - 共 - 二乙烯基苯）连续棒上的反相色谱分析
Reversed-phase chromatography of small molecules and peptides on a continuous rod of macroporous poly(styrene-co-divinylbenzene).
作者信息
Wang Q C, Svec F, Fréchet J M
机构信息
Cornell University, Department of Chemistry, Baker Laboratory, Ithaca, NY 14853-1301.
出版信息
J Chromatogr A. 1994 May 27;669(1-2):230-5. doi: 10.1016/0021-9673(94)80352-8.
PMID:8055104
Abstract
A continuous "molded" rod of porous poly(styrene-co-divinylbenzene) prepared by a bulk free radical polymerization within the confines of a chromatographic column has been used successfully for the reversed-phase HPLC of alkylbenzenes and peptides. An excellent rapid separation of bradykinin and [D-Phe7]-bradykinin with a molecular mass of about 1000 was also achieved.
摘要
通过在色谱柱范围内进行本体自由基聚合制备的连续“模塑”多孔聚（苯乙烯 - 共 - 二乙烯基苯）棒已成功用于烷基苯和肽的反相高效液相色谱分析。还实现了对分子量约为1000的缓激肽和[D - Phe7] - 缓激肽的出色快速分离。
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