Han G R, Wang Y D, Feng L, Liu Z Q, Zhang H B
Hebei Provincial Institute for Drug Control, Shijiazhuang.
Zhongguo Zhong Yao Za Zhi. 1993 Feb;18(2):93-5, 126.
In the paper systematic studies on quality standards for Qingwei Huanglian Pills are reported, along with the TLC identification of Gardenia jasminoides, Scutellaria baicalensis and Anemarrhena asphodeloides and the quantitative determination of berberine in Coptis chinensis and Phellodendron chinese by TLC densitometric method. To simplify the operation, the same solvent was used for both the identification and determination. The quantitative method is simple, sensitive, reproducible and accurate. The recovery of berberine is 99.48%. The coefficient of variation is 1.42%.
本文报道了对清胃黄连丸质量标准的系统研究,包括栀子、黄芩和知母的薄层色谱鉴别以及用薄层扫描法对黄连和黄柏中黄连素的定量测定。为简化操作,鉴别和测定采用同一溶剂。该定量方法简便、灵敏、重现性好、准确。黄连素的回收率为99.48%,变异系数为1.42%。