• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利:CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法,用中文像聊天一样搜索,搜遍4000万医学文献。AI智能推荐,让科研检索更轻松。

立即免费搜索

文件翻译

保留排版,准确专业,支持PDF/Word/PPT等文件格式,支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述,25分钟生成高质量综述,智能提取关键信息,辅助科研写作。

立即免费体验

Enantiomeric resolution by HPLC of axial chiral amides using amylose tris[(S)-1-phenylethylcarbamate].

作者信息

Cass Q B, Degani A L, Tiritan M E, Matlin S A, Curran D P, Balog A

机构信息

Departamento de Química, Universidade Federal de São Carlos, Brazil.

出版信息

Chirality. 1997;9(2):109-12. doi: 10.1002/(SICI)1520-636X(1997)9:2<109::AID-CHIR6>3.0.CO;2-C.

DOI:10.1002/(SICI)1520-636X(1997)9:2<109::AID-CHIR6>3.0.CO;2-C
PMID:9134693
Abstract

The enantiomeric resolution of a series of N-arylamides was examined on amylose tris[(S)-1-phenylethylcarbamate] coated onto aminopropylated 7 microns silica with 500 A diameter pores and on naked silica 5 microns particle size with 500 A diameter pores. The enantiomeric resolution obtained for this series was excellent on both columns. The enantioselectivity of cellulose and amylose tris(3,5-dimethylphenylcarbamate) coated onto APS-Hypersil (120 A pore size, 5 microns particle size) was also investigated for this series of compounds.

摘要

相似文献

1
Enantiomeric resolution by HPLC of axial chiral amides using amylose tris[(S)-1-phenylethylcarbamate].
Chirality. 1997;9(2):109-12. doi: 10.1002/(SICI)1520-636X(1997)9:2<109::AID-CHIR6>3.0.CO;2-C.
2
Enantiomeric resolution of kielcorin derivatives by HPLC on polysaccharide stationary phases using multimodal elution.使用多峰洗脱在多糖固定相上通过高效液相色谱法拆分基尔考林衍生物的对映体。
Chirality. 2004 May 15;16(5):279-85. doi: 10.1002/chir.20031.
3
Immobilized versus coated amylose tris(3,5-dimethylphenylcarbamate) chiral stationary phases for the enantioselective separation of cyclopropane derivatives by liquid chromatography.用于通过液相色谱对环丙烷衍生物进行对映体选择性分离的固定化与涂覆直链淀粉三(3,5-二甲基苯基氨基甲酸酯)手性固定相。
J Chromatogr A. 2006 Jan 6;1101(1-2):171-8. doi: 10.1016/j.chroma.2005.09.081. Epub 2005 Oct 24.
4
High-performance liquid chromatographic enantioseparations on capillary columns containing monolithic silica modified with amylose tris(3,5-dimethylphenylcarbamate).在含有用直链淀粉三(3,5-二甲基苯基氨基甲酸酯)改性的整体硅胶的毛细管柱上进行高效液相色谱对映体分离。
J Chromatogr A. 2006 Mar 31;1110(1-2):46-52. doi: 10.1016/j.chroma.2006.01.076. Epub 2006 Feb 14.
5
Chiral recognition ability and solvent versatility of bonded amylose tris(3,5-dimethylphenylcarbamate) chiral stationary phase: enantioselective liquid chromatographic resolution of racemic N-alkylated barbiturates and thalidomide analogs.键合直链淀粉三(3,5-二甲基苯基氨基甲酸酯)手性固定相的手性识别能力和溶剂通用性:外消旋N-烷基化巴比妥酸盐和沙利度胺类似物的对映体选择性液相色谱分离
Chirality. 2007 Jun;19(6):477-84. doi: 10.1002/chir.20398.
6
Enantioseparations using nonaqueous capillary electrochromatography on cellulose and amylose tris(3,5-dimethylphenylcarbamates) coated on silica gels of various pore and particle size.使用涂覆在各种孔径和粒径硅胶上的纤维素和直链淀粉三(3,5-二甲基苯基氨基甲酸酯)通过非水毛细管电色谱进行对映体拆分。
Electrophoresis. 2001 Apr;22(7):1282-91. doi: 10.1002/1522-2683(200105)22:7<1282::AID-ELPS1282>3.0.CO;2-Y.
7
An improved and validated LC method for resolution of bicalutamide enantiomers using amylose tris-(3,5-dimethylphenylcarbamate) as a chiral stationary phase.一种经过改进和验证的液相色谱(LC)方法,该方法使用直链淀粉三(3,5-二甲基苯基氨基甲酸酯)作为手性固定相来拆分比卡鲁胺对映体。
J Pharm Biomed Anal. 2006 Sep 26;42(3):347-53. doi: 10.1016/j.jpba.2006.04.014. Epub 2006 Jun 5.
8
Enantioseparations on amylose tris(5-chloro-2-methylphenylcarbamate) in nano-liquid chromatography and capillary electrochromatography.在纳米液相色谱和毛细管电色谱中,直链淀粉三(5-氯-2-甲基苯甲氨基甲酸酯)的对映体分离。
J Chromatogr A. 2010 Feb 12;1217(7):1166-74. doi: 10.1016/j.chroma.2009.09.024. Epub 2009 Sep 12.
9
Enantioseparation of 2-aryl-1,3-dicarbonyl analogues by high performance liquid chromatography using polysaccharide type chiral stationary phase.使用多糖类手性固定相通过高效液相色谱法对2-芳基-1,3-二羰基类似物进行对映体拆分。
Chirality. 2008 Feb;20(2):147-50. doi: 10.1002/chir.20513.
10
Immobilized polysaccharide derivatives: chiral packing materials for efficient HPLC resolution.固定化多糖衍生物:用于高效液相色谱分离的手性填充材料。
Chem Rec. 2007;7(2):91-103. doi: 10.1002/tcr.20107.

引用本文的文献

1
Strategies for Preparation of Chiral Stationary Phases: Progress on Coating and Immobilization Methods.手性固定相的制备策略:涂层和固定化方法的进展。
Molecules. 2021 Sep 9;26(18):5477. doi: 10.3390/molecules26185477.
2
Chiral Stationary Phases for Liquid Chromatography: Recent Developments.手性固定相在液相色谱中的应用:最新进展。
Molecules. 2019 Feb 28;24(5):865. doi: 10.3390/molecules24050865.