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关于在氮化硅表面等离子喷涂生物活性陶瓷作为复合骨内植入物的研究。

Study on plasma-spraying coating bioactive ceramics onto silicon nitride surface as composite endosteal implants.

作者信息

Xu L L, Shi S J

机构信息

Department of Prosthodontics, Stomatological Hospital, Tianjin Medical University, P.R. China.

出版信息

Biomed Sci Instrum. 1997;33:585-9.

PMID:9731426
Abstract

The successful key of endosteal implants depends on the properties of implant materials which are very important for oral implantology at the present. Because silicon nitride has high strength and hydroxylapatite (HA) and flourapatite (FA) have good biocompatibility. In this paper, we apply silicon nitride as base material. Plasma spray HA, FA onto its surface as composite endosteal implants. Physical and chemical properties test, includes X-ray diffraction (XRD), scanning electronic microscope (SEM), EDAX and bonding strength test (push-out test). The results indicate: after plasma-spraying coating, crystalline phase of HA and FA unchanged and form a lot of pores among the crystal particles. Those pores benefit bone growing into them. It is very important for implants to be fixed in bone for long time, Ca/P ratio has no significant change. Bonding strength test results indicate: Si3N4-HA 23.6MPa, Si3N4-FA 27.12 MPa are higher than that of Ti-HA 15.07 MPa. On the basis of these studies, they are kinds of ideal implant materials.

摘要

骨内植入物成功的关键取决于植入材料的性能,目前这些性能对口腔种植学非常重要。因为氮化硅具有高强度,而羟基磷灰石(HA)和氟磷灰石(FA)具有良好的生物相容性。在本文中,我们将氮化硅用作基础材料。通过等离子喷涂将HA、FA涂覆在其表面,制成复合骨内植入物。进行物理和化学性能测试,包括X射线衍射(XRD)、扫描电子显微镜(SEM)、能谱分析(EDAX)和结合强度测试(推出试验)。结果表明:等离子喷涂涂层后,HA和FA的晶相未发生变化,且在晶体颗粒之间形成了许多孔隙。这些孔隙有利于骨长入其中。对于植入物在骨中长期固定非常重要,钙磷比没有显著变化。结合强度测试结果表明:Si3N4-HA为23.6MPa,Si3N4-FA为27.12MPa,高于Ti-HA的15.07MPa。基于这些研究,它们是理想的植入材料。

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