Phrukkanon S, Burrow M F, Tyas M J
University of Melbourne, School of Dental Science, Melbourne, Australia.
Dent Mater. 1998 Mar;14(2):120-8. doi: 10.1016/s0109-5641(98)00018-9.
This study was conducted to determine the effect of the bonding area on the micro-shear and micro-tensile bond strengths of four dentin adhesive systems (Scotchbond MP Plus, 3M Dental Products, St. Paul, MN; OptiBond FL, Kerr Corp., Orange, CA; OptiBond Solo, Kerr Corp., Orange, CA; One-Step, Bisco, Inc., Itasca, IL).
Sixty extracted human molars were cut vertically and occlusal enamel removed, one half of the tooth was used for tensile testing and one half for shear. The occlusal dentin was bonded according to manufacturers' directions with a resin composite block and sectioned to obtain up to three square bar-shaped specimens, which were shaped with a high speed diamond bur on a lathe to produce cylindrical specimens of 1.2, 1.4 or 2.0 mm diameter at the bonded interface. The bonds were stressed in shear or tension at a crosshead speed of 1 mm min-1. The mean bond strengths were compared using one-way ANOVA, two-way ANOVA and Student's t-test. The fractured surfaces were examined under a scanning electron microscope and the frequency of fracture modes was compared using the Kruskal-Wallis and Mann-Whitney U tests.
For all materials, the 2.0 mm diameter group showed significantly lower bond strengths than the 1.2 mm diameter group in both shear and tensile tests (p < 0.05). Most specimens of 1.2 mm or 1.4 mm diameter exhibited adhesive failure at the interface between the dentin and the adhesive resin.
The results indicate that small surface areas of test specimens are associated with higher bond strengths and that the effect on tensile and shear values is similar.
本研究旨在确定粘结面积对四种牙本质粘结系统(Scotchbond MP Plus,3M牙科产品公司,明尼苏达州圣保罗市;OptiBond FL,克尔公司,加利福尼亚州奥兰治市;OptiBond Solo,克尔公司,加利福尼亚州奥兰治市;One-Step,必思科公司,伊利诺伊州伊塔斯卡市)微剪切和微拉伸粘结强度的影响。
将60颗拔除的人类磨牙垂直切割并去除咬合面釉质,牙齿的一半用于拉伸测试,另一半用于剪切测试。按照制造商的说明,用树脂复合材料块粘结咬合面牙本质,然后切片以获得多达三个方形棒状标本,在车床上用高速金刚石车针将其加工成粘结界面处直径为1.2、1.4或2.0 mm的圆柱形标本。以1 mm/min的十字头速度对粘结处施加剪切或拉伸应力。使用单因素方差分析、双因素方差分析和学生t检验比较平均粘结强度。在扫描电子显微镜下检查断裂表面,并使用Kruskal-Wallis检验和Mann-Whitney U检验比较断裂模式的频率。
对于所有材料,在剪切和拉伸测试中,直径2.0 mm组的粘结强度均显著低于直径1.2 mm组(p < 0.05)。大多数直径为1.2 mm或1.4 mm的标本在牙本质与粘结树脂之间的界面处表现出粘结失败。
结果表明,测试标本的小表面积与较高的粘结强度相关,并且对拉伸和剪切值的影响相似。