药品中糖精的葡萄糖测定法。
GLC determination of saccharin in pharmaceutical products.
作者信息
Ratchik E M, Viswanathan V
出版信息
J Pharm Sci. 1975 Jan;64(1):133-5. doi: 10.1002/jps.2600640131.
PMID:1133688
Abstract
A GLC method was developed for the assay of saccharin in pharmaceutical products. The procedure requires silylation with N, O-bis (trimethylsily) acetamide and subsequent chromatography on trifluoropropyl methyl silicone, using n-octacosane as an internal standard.
摘要
开发了一种用于测定药品中糖精的气相色谱法。该方法需要用N，O-双（三甲基硅基）乙酰胺进行硅烷化，然后以正二十八烷为内标，在三氟丙基甲基硅氧烷上进行色谱分析。
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