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有或无湿气的酸蚀系统及自酸蚀底漆系统所形成的树脂-牙釉质界面的牙釉质拉伸粘结强度及形态

Enamel tensile bond strength and morphology of resin-enamel interface created by acid etching system with or without moisture and self-etching priming system.

作者信息

Torii Y, Itou K, Hikasa R, Iwata S, Nishitani Y

机构信息

Department of Operative Dentistry, Okayama University Dental School, Japan.

出版信息

J Oral Rehabil. 2002 Jun;29(6):528-33. doi: 10.1046/j.1365-2842.2002.00855.x.

DOI:10.1046/j.1365-2842.2002.00855.x
PMID:12071920
Abstract

The purpose of this study was to estimate the effect of three types of different adhesive systems on enamel adhesion. Scotchbond Multi-Purpose (MP) as a traditional system, Single Bond (SB) as a wet-bonding system and Clearfil SE Bond (SE) and Unifil Bond (UB) as self-etching priming systems were used. Bovine enamel was treated with each system and tensile bond strength (TBS) of resin to the enamel was measured. The conditioned enamel surfaces and resin-enamel interfaces were also morphologically observed with scanning electron microscope (SEM). The mean TBS for MP, SB, SE and UB were 15.3, 13.7, 14.3 and 11.6 MPa, respectively. There was no significant difference in mean TBS among all products but the traditional system showed the most stable TBS. In SEM observations, self-etching primer created a weaker etched pattern on the enamel surface than phosphoric acid. At the resin-enamel interfaces, thick tag-like extensions penetrated into the enamel etched with phosphoric acid regardless of using the wet-bonding technique, while self-etching primer created thin lamina-like resin penetrations. These results indicate that the traditional system with phosphoric acid etching exhibits the most stable enamel adhesion although the enamel-bonding promoting abilities of these adhesive systems are equivalent to each other.

摘要

本研究的目的是评估三种不同粘接系统对牙釉质粘接的影响。使用Scotchbond多功能(MP)作为传统系统,单组分粘接剂(SB)作为湿粘接系统,以及Clearfil SE Bond(SE)和Unifil Bond(UB)作为自酸蚀底漆系统。用每种系统处理牛牙釉质,并测量树脂与牙釉质之间的拉伸粘接强度(TBS)。还用扫描电子显微镜(SEM)对处理后的牙釉质表面和树脂-牙釉质界面进行了形态学观察。MP、SB、SE和UB的平均TBS分别为15.3、13.7、14.3和11.6MPa。所有产品的平均TBS之间没有显著差异,但传统系统显示出最稳定的TBS。在SEM观察中,自酸蚀底漆在牙釉质表面产生的蚀刻图案比磷酸弱。在树脂-牙釉质界面处,无论使用湿粘接技术如何,厚的标签状延伸物都会穿透用磷酸蚀刻的牙釉质,而自酸蚀底漆则产生薄的层状树脂渗透。这些结果表明,尽管这些粘接系统促进牙釉质粘接的能力彼此相当,但采用磷酸蚀刻的传统系统表现出最稳定的牙釉质粘接。

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Enamel tensile bond strength and morphology of resin-enamel interface created by acid etching system with or without moisture and self-etching priming system.有或无湿气的酸蚀系统及自酸蚀底漆系统所形成的树脂-牙釉质界面的牙釉质拉伸粘结强度及形态
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Dent J (Basel). 2021 Nov 20;9(11):138. doi: 10.3390/dj9110138.
2
Microleakage of pit and fissure sealings placed after enamel conditioning with phosphoric acid or with self-etching primers/adhesives.磷酸酸蚀处理或自酸蚀处理后窝沟封闭的微渗漏。
Clin Exp Dent Res. 2021 Oct;7(5):763-771. doi: 10.1002/cre2.420. Epub 2021 Apr 7.
3
Improvement of enamel bond strengths for conventional and resin-modified glass ionomers: acid-etching vs. conditioning.
提高传统型和树脂改良型玻璃离子水门汀的釉质粘结强度:酸蚀与预处理。
J Zhejiang Univ Sci B. 2013 Nov;14(11):1013-24. doi: 10.1631/jzus.B1300034.
4
Repeated bonding of fixed retainer increases the risk of enamel fracture.固定保持器的反复粘结会增加牙釉质骨折的风险。
Odontology. 2014 Jan;102(1):89-97. doi: 10.1007/s10266-012-0095-9. Epub 2012 Dec 14.
5
In vitro evaluation of self-etch bonding in orthodontics using cyclic fatigue.体外评估正畸自酸蚀粘接剂的循环疲劳性能。
Angle Orthod. 2011 Sep;81(5):783-7. doi: 10.2319/012811-59.1. Epub 2011 May 5.
6
SEM analysis of the acid-etched enamel patterns promoted by acidic monomers and phosphoric acids.酸性单体和磷酸促进的酸蚀牙釉质模式的扫描电子显微镜分析。
J Appl Oral Sci. 2006 Dec;14(6):427-35. doi: 10.1590/s1678-77572006000600008.
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Adhesion after erbium, chromium:yttrium-scandium-gallium-garnet laser application at three different irradiation conditions.铒铬:钇钪镓石榴石激光在三种不同照射条件下应用后的粘连情况。
Lasers Med Sci. 2009 Jan;24(1):67-73. doi: 10.1007/s10103-007-0521-3. Epub 2007 Nov 20.
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Scanning electron microscopy and energy-dispersive X-ray analysis of self-etching adhesive systems to ground and unground enamel.自酸蚀粘结系统对酸蚀和未酸蚀牙釉质的扫描电子显微镜及能量色散X射线分析
J Mater Sci Mater Med. 2007 Jun;18(6):1111-6. doi: 10.1007/s10856-007-0149-7. Epub 2007 Feb 1.