Wang S X, Hua H M, Wu L J, Li X, Zhu T R
Research Department of Natural Drugs, Shenyang College of Pharmacy.
Yao Xue Xue Bao. 1992;27(10):743-7.
Seven anthraquinones were isolated from the ethyl alcohol extracts of the roots of Rubia Cordifolia L. By means of spectrometric data combined with physico-chemical properties, six of them were identified as 2-methyl-1,3,6-trihydroxy-9,10-anthraquinone (I), 1-hydroxy-9,10-anthraquinone(II), 1,2,4-trihydroxy-9,10-anthrequinone(III), 2-methyl-1,3,6-trihydroxy-9,10-anthraquinone-3-O-beta-D-glucoside(IV), 1,2-dijhydroxy-9,10-anthraquinone-2-O-beta-D-xylosyl(1-->6)-beta-D -glucoside(V) and 1,3-dihydroxy-2-hydroxymethyl1-9,10-anthraquinone-3-O-beta-D- xylosyl(1-->6)-beta-D-glucoside(VI). VII is a new compound. Its structure was elucidated to be 2-methyl-1,3,6-trihydroxy-9,10-anthraquinone-3-O-beta-D-xylosyl(1-->2)-b eta-D- (6'-O-acetyl)glucoside.
从茜草根部的乙醇提取物中分离出七种蒽醌。借助光谱数据并结合物理化学性质,其中六种被鉴定为2-甲基-1,3,6-三羟基-9,10-蒽醌(I)、1-羟基-9,10-蒽醌(II)、1,2,4-三羟基-9,10-蒽醌(III)、2-甲基-1,3,6-三羟基-9,10-蒽醌-3-O-β-D-葡萄糖苷(IV)、1,2-二羟基-9,10-蒽醌-2-O-β-D-木糖基(1→6)-β-D-葡萄糖苷(V)和1,3-二羟基-2-羟甲基-9,10-蒽醌-3-O-β-D-木糖基(1→6)-β-D-葡萄糖苷(VI)。VII是一种新化合物。其结构经鉴定为2-甲基-1,3,6-三羟基-9,10-蒽醌-3-O-β-D-木糖基(1→2)-β-D-(6'-O-乙酰基)葡萄糖苷。