Rahiotis Chris, Kakaboura Afrodite, Loukidis Michalis, Vougiouklakis George
Biomaterials Laboratory, University of Athens, Greece.
Eur J Oral Sci. 2004 Feb;112(1):89-94. doi: 10.1111/j.0909-8836.2004.00092.x.
This study compared monomer conversion (DC), the per cent linear polymerization shrinkage (%LS), the wall-to-wall contraction pattern (per cent of peripheral opening, %DM, and maximal marginal gap, MG) and depth of cure (DOC), of a hybrid resin composite (Spectrum TPH) exposed to different types of light-curing units and exposure modes (Virtuoso-PAC, Elipar TriLight-QTH, and FreeLight-LED). The QTH and LED units were used in two curing modes: the exponential ramp and the continuous output modes. Monomer conversion was investigated by micro Multiple Internal Reflection (MIR)-Fourier-transform infrared (FTIR) spectroscopy and %LS was measured by the deflective disc method. The wall-to-wall contraction method used a cylindrical cavity model in extracted human teeth. The per cent debonded margins relative to the cavity periphery (%DM) and the width of maximum gap (MG) was evaluated. The DOC was determined using Vickers microhardness measurements (200 g load, 20 s) at the top surface (H0), at 2 mm (H2) and at 4 mm (H4) depths, and the results expressed as H2/H0 and H4/H0 ratios. Significantly lower %DC and %LS values were provided by PAC and LED units. No differences were found in %DM among the curing units and PAC exhibited the highest MG. No significant differences were noted among light-curing groups in terms of H2/H0 microhardness values. The QTH, operated in exponential mode, resulted in the highest H4/H0 value. The exponential mode of the QTH demonstrated superior performance for the total of the characteristics evaluated.
本研究比较了一种混合树脂复合材料(Spectrum TPH)在不同类型光固化设备及曝光模式(Virtuoso-PAC、Elipar TriLight-QTH和FreeLight-LED)下的单体转化率(DC)、线性聚合收缩率(%LS)、壁对壁收缩模式(周边开口百分比、%DM和最大边缘间隙,MG)以及固化深度(DOC)。QTH和LED设备采用两种固化模式:指数斜坡模式和连续输出模式。通过显微多重内反射(MIR)-傅里叶变换红外(FTIR)光谱法研究单体转化率,采用偏转圆盘法测量%LS。壁对壁收缩法使用拔除的人牙中的圆柱形腔模型。评估相对于腔周边的脱粘边缘百分比(%DM)和最大间隙宽度(MG)。使用维氏显微硬度测量(200 g载荷,20 s)在顶面(H0)、2 mm深度(H2)和4 mm深度(H4)处测定DOC,结果以H2/H0和H4/H0比值表示。PAC和LED设备提供的%DC和%LS值显著较低。各固化设备之间的%DM没有差异,PAC的MG最高。在光固化组之间,就H2/H0显微硬度值而言,未发现显著差异。以指数模式运行的QTH产生最高的H4/H0值。QTH的指数模式在所有评估特征方面表现出卓越性能。