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粉液混合比对牙科陶瓷孔隙率和半透明度的影响。

Influence of powder/liquid mixing ratio on porosity and translucency of dental porcelains.

作者信息

Zhang Yunlong, Griggs Jason A, Benham Adam W

机构信息

Department of Biomaterials Science, Baylor College of Dentistry, Dallas, TX 75246, USA.

出版信息

J Prosthet Dent. 2004 Feb;91(2):128-35. doi: 10.1016/j.prosdent.2003.10.014.

Abstract

STATEMENT OF PROBLEM

Dental technicians use a variety of techniques when condensing dental porcelains. It is unclear whether these techniques affect the total porosity and translucency of dental porcelains.

PURPOSE

The objective of this study was to determine whether varying the powder/liquid ratio during condensation affects porosity and translucency of porcelains. Material and methods Duceram LFC dentin, Duceram LFC incisal, IPS Eris dentin, and IPS Eris incisal porcelains were studied. For each specimen, 1.0 g of porcelain powder was mixed with 1 of 3 different volumes of deionized water to form a slurry with a thin, medium, or thick consistency. The slurries were condensed in a plastic syringe mold, fired, and polished to a 3-microm finish to form 12 groups of 4 specimens each (14-mm diameter, 1.10-mm thickness). The apparent density (g/mL) of each specimen was measured using Archimedes method, and the porosity (%) calculated. Each specimen was coupled to standard ceramic tiles using an immersion liquid, and the color shade was measured in CIE Yxy coordinates using a tristimulus colorimeter. Translucency was assessed by calculating the contrast ratio of shade value (Y) in front of black versus white backgrounds. Two-way analysis of variance and Tukey's multiple comparison tests (alpha = .05) were used to test for significant effects of factors.

RESULTS

Porcelain type and powder/liquid ratio had a significant interactive effect on the apparent density (P < .001) and on total porosity (P = .003); however, there was no consistent trend. The powder/liquid ratio did not significantly affect translucency (P = .28), but porcelain type had a significant effect on translucency (P < .001).

CONCLUSION

In this in vitro study, total porosity of specimens prepared using 4 porcelains was found to be sensitive to powder/liquid ratio; whereas translucency was found to be insensitive to powder/liquid ratio.

摘要

问题陈述

牙科技术人员在压实牙科瓷粉时会使用多种技术。目前尚不清楚这些技术是否会影响牙科瓷粉的总孔隙率和透明度。

目的

本研究的目的是确定在压实过程中改变粉液比对瓷粉的孔隙率和透明度的影响。材料与方法研究了Duceram LFC牙本质瓷、Duceram LFC切端瓷、IPS Eris牙本质瓷和IPS Eris切端瓷。对于每个样本,将1.0 g瓷粉与3种不同体积的去离子水之一混合,形成稀、中、稠三种稠度的浆料。将浆料在塑料注射器模具中压实、烧制并抛光至3微米的光洁度,以形成12组,每组4个样本(直径14毫米,厚度1.10毫米)。使用阿基米德法测量每个样本的表观密度(克/毫升),并计算孔隙率(%)。使用浸没液将每个样本与标准瓷砖耦合,并使用三色刺激色度计以CIE Yxy坐标测量颜色深浅。通过计算黑色与白色背景前的色度值(Y)的对比度来评估透明度。使用双向方差分析和Tukey多重比较检验(α = 0.05)来检验因素的显著影响。

结果

瓷粉类型和粉液比对表观密度(P < 0.001)和总孔隙率(P = 0.003)有显著的交互作用;然而,没有一致的趋势。粉液比对透明度没有显著影响(P = 0.28),但瓷粉类型对透明度有显著影响(P < 0.001)。

结论

在这项体外研究中,发现使用4种瓷粉制备的样本的总孔隙率对粉液比敏感;而透明度对粉液比不敏感。

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