Mohamed-Tahir M A, Yap A U J
Department of Preventive Dentistry, Faculty of Dentistry, National University of Singapore, Republic of Singapore.
Oper Dent. 2004 Sep-Oct;29(5):586-91.
This study determined the effect of pH on the surface texture of commonly used posterior glass-ionomer based/containing restorative materials. The materials evaluated included a compomer (Dyract AP), a giomer (Beautifil) and two highly viscous glass ionomer cements (Fuji IX and Ketac Molar). A resin composite (Esthet-X) was used for comparison. Forty-two specimens (3-mm wide x 3-mm long x 2-mm deep) were made for each material. The specimens were divided into six groups and conditioned in the following solutions at 37 degrees C for one week: Citric acid (pH 2, 3, 4, 5 and 6) and distilled water (pH 7). After conditioning, the surface roughness (Ra, microm) of each specimen was measured using a surface profilometer (Surftest, Mitutoyo Corp, Tokyo, Japan). Data was analyzed using one-way ANOVA and Scheffe's test at a significance level of 0.05. The effects of pH on the surface texture of glass-ionomer based/containing restoratives were material dependent. Ra values ranged from 0.02 microm to 0.15 microm and 0.03 microm to 4.40 microm for pH 7 and 2, respectively. With the exception of the composite, the surface roughness of all materials evaluated was significantly affected by acids of low pH. The surface texture of highly viscous glass ionomer cements deteriorated significantly when conditioned in solutions of low pH, which makes them more susceptible to clinical failure.
本研究确定了pH值对常用的基于玻璃离子体/含玻璃离子体的修复材料表面质地的影响。所评估的材料包括一种复合体(Dyract AP)、一种聚酸改性复合树脂(Beautifil)和两种高粘性玻璃离子水门汀(Fuji IX和Ketac Molar)。使用一种树脂复合材料(Esthet-X)作为对照。每种材料制作42个试件(宽3毫米×长3毫米×深2毫米)。将试件分为六组,并在37摄氏度下于下列溶液中处理一周:柠檬酸(pH值2、3、4、5和6)和蒸馏水(pH值7)。处理后,使用表面轮廓仪(日本东京三丰公司的Surftest)测量每个试件的表面粗糙度(Ra,微米)。使用单向方差分析和谢费检验对数据进行分析,显著性水平为0.05。pH值对基于玻璃离子体/含玻璃离子体的修复材料表面质地的影响因材料而异。对于pH值7和2,Ra值分别在0.02微米至0.15微米和0.03微米至4.40微米范围内。除了复合材料外,所有评估材料的表面粗糙度都受到低pH值酸的显著影响。高粘性玻璃离子水门汀在低pH值溶液中处理时表面质地显著恶化,这使其更容易出现临床失败。