Schlepütz C M, Herger R, Willmott P R, Patterson B D, Bunk O, Brönnimann Ch, Henrich B, Hülsen G, Eikenberry E F
Swiss Light Source, Paul Scherrer Institute, CH-5232 Villigen, Switzerland.
Acta Crystallogr A. 2005 Jul;61(Pt 4):418-25. doi: 10.1107/S0108767305014790. Epub 2005 Jun 23.
The use of an area detector in grazing-incidence X-ray experiments lends many advantages in terms of both speed and reliability. Here a discussion is given of the procedures established using the PILATUS pixel detector developed at the Swiss Light Source for optimizing data acquisition and analysis of surface diffraction data at the Materials Science beamline, especially with regard to reflectivity measurements, crystal truncation and fractional order rods, and grazing-incidence diffraction experiments.
在掠入射X射线实验中使用面探测器在速度和可靠性方面都具有诸多优势。本文讨论了利用瑞士光源研发的PILATUS像素探测器所建立的程序,以优化材料科学光束线处表面衍射数据的数据采集与分析,特别是在反射率测量、晶体截断和分数阶棒以及掠入射衍射实验方面。