Li Yu, Liu Minrui
School of Chemistry and Chemical Engineering, Sun Yat-Sen University, Guangzhou 510275.
Zhong Yao Cai. 2005 Apr;28(4):330-2.
A new method of microwave extraction was used to extract the yellow pigment from Rabdosia serra (Maxim.) Hara. The extraction processes were investigated and the optimal conditions were determined as follows: raw material is 2. 0000 g dry powder, the extraction agent is 95% alcohol, the ratio of raw material to extraction agent is 1:60 (g:ml) , microwave power is 464 W, extraction time is 350 s, extraction times is 3. Under the optimal conditions, extraction rate is 90.6%, productive rate is 12.7%, colority E (1%, 330 nm) is 53.3 and pH value of the extractive is 6.0. Compared with solvent extraction, microwave extraction reduces extraction time from 6 h to 350 s and increases extraction rate from 90.4% to 90.6%.
采用一种新的微波萃取方法从溪黄草中提取黄色素。对萃取工艺进行了研究,并确定了最佳条件如下:原料为2.0000 g干粉,萃取剂为95%乙醇,原料与萃取剂的比例为1:60(g:ml),微波功率为464 W,萃取时间为350 s,萃取次数为3次。在最佳条件下,萃取率为90.6%,得率为12.7%,提取物的色度E(1%,330 nm)为53.3,提取物的pH值为6.0。与溶剂萃取相比,微波萃取将萃取时间从6小时缩短至350秒,萃取率从90.4%提高到90.6%。