Mutal L, Gani O
Department of Endodontics, Faculty of Dentistry, National University of Córdoba, Córdoba, Argentina.
Int Endod J. 2005 Oct;38(10):690-6. doi: 10.1111/j.1365-2591.2005.00988.x.
To assess qualitatively the presence of pores and vacuoles in the structure of various endodontic sealers when set.
Eight specimens were prepared in keeping with Instituto Argentino de Racionalización de Materiales (IRAM) and ISO regulations for each of the 10 sealers assessed. Four specimens per sealer were examined to identify the presence of structural defects, termed pores, on the external surface. The remaining four specimens were used to examine the presence of defects on the surface exposed by cross-sectional fracture; these were termed vacuoles. The largest and smallest diameters of the pores and vacuoles were measured by scanning electron microscope on both surfaces. The structural defects were classified according to their frequency as abundant, frequent, scarce or exceptional.
Pores and vacuoles were consistently found in every specimen of each sealer. However, their frequency and dimensions were greater in zinc-eugenol-based sealers than in epoxy-resins and glass-ionomer sealers; they increased if the sealer contained calcium hydroxide. The diameter of the pores ranged from 5 to 320 microm and the diameter of the vacuoles ranged from 80 to 500 microm. The diameter of the vacuoles always exceeded that of the pores.
Pores and vacuoles were a consistent finding in set sealers. Their frequency and size depended on the density of the sealer and increased when the sealers contained calcium hydroxide.
定性评估各种根管封闭剂凝固后结构中孔隙和空泡的存在情况。
按照阿根廷材料合理化协会(IRAM)和ISO规范,为所评估的10种封闭剂中的每一种制备8个标本。每种封闭剂取4个标本检查其外表面是否存在称为孔隙的结构缺陷。其余4个标本用于检查横断面断裂后暴露表面的缺陷情况,这些缺陷称为空泡。通过扫描电子显微镜测量两个表面上孔隙和空泡的最大和最小直径。根据结构缺陷的出现频率将其分类为丰富、频繁、稀少或罕见。
在每种封闭剂的每个标本中均始终发现孔隙和空泡。然而,与环氧树脂和玻璃离子封闭剂相比,基于氧化锌丁香酚的封闭剂中孔隙和空泡的出现频率和尺寸更大;如果封闭剂含有氢氧化钙,其频率和尺寸会增加。孔隙直径范围为5至320微米,空泡直径范围为80至500微米。空泡直径始终超过孔隙直径。
孔隙和空泡在凝固后的封闭剂中是一致的发现。它们的出现频率和大小取决于封闭剂的密度,并且当封闭剂含有氢氧化钙时会增加。