Algera Tjalling J, Kleverlaan Cornelis J, Prahl-Andersen Birte, Feilzer Albert J
Department of Orthodontics, Academic Centre for Dentistry Amsterdam (ACTA), Universiteit van Amsterdam and Vrije Universiteit, Amsterdam 1066 EA, The Netherlands.
Dent Mater. 2006 Sep;22(9):852-6. doi: 10.1016/j.dental.2005.11.013. Epub 2006 Jan 10.
Aim of this study was to investigate the influence of temperature on the setting time and compressive strength of two conventional glass-ionomer cements (GIC's) and to determine the influence of storage medium, oil or water and storage time.
Two conventional GIC's, Ketac Molar (3 M-ESPE Dental Products, Seefeld, Germany) and Fuji IX Fast (GC Corp., Tokyo, Japan) were used to perform flow property tests and compression tests. Flow property measurements were performed using a displacement rheometer at six different temperatures. From the results of the rheometer tests, the working times and setting times could be determined. The samples for the compressive tests were stored at four different temperatures and in two different media. Testing took place at five time intervals reaching from 1 h to 3 months.
The results of rheometer tests showed that a temperature increase speeded up the setting reaction significantly. The compressive strength results showed a jump in time as a result of the higher curing temperature but no long-term strength effect was observed. Materials curing in oil reached a significantly higher compressive strength compared to storage in water and Fuji IX Fast is significantly stronger than Ketac Molar.
It was concluded that a temperature between 333 and 343 K almost sets conventional GIC's on command and improves the early compressive strength.
本研究旨在探讨温度对两种传统玻璃离子水门汀(GIC)凝固时间和抗压强度的影响,并确定储存介质(油或水)及储存时间的影响。
使用两种传统GIC,即Ketac Molar(德国赛费尔德3M-ESPE牙科产品公司)和Fuji IX Fast(日本东京GC公司)进行流动性测试和压缩测试。使用位移流变仪在六个不同温度下进行流动性测量。根据流变仪测试结果可确定工作时间和凝固时间。用于压缩测试的样品在四个不同温度和两种不同介质中储存。测试在从1小时到3个月的五个时间间隔进行。
流变仪测试结果表明,温度升高显著加快了凝固反应。抗压强度结果显示,较高的固化温度导致强度在时间上有跃升,但未观察到长期强度效应。与在水中储存相比,在油中固化的材料达到的抗压强度显著更高,且Fuji IX Fast比Ketac Molar显著更强。
得出的结论是,333至343K之间的温度几乎可按需使传统GIC凝固,并提高早期抗压强度。