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使用乙醇钠蚀刻和硅烷/粘合剂组合偶联提高石英纤维桩核粘结质量。

Improving the quality of the quartz fiber postcore bond using sodium ethoxide etching and combined silane/adhesive coupling.

作者信息

Monticelli Francesca, Osorio Raquel, Toledano Manuel, Goracci Cecilia, Tay Franklin R, Ferrari Marco

机构信息

Department of Restorative Dentistry and Dental Materials, University of Siena, Italy.

出版信息

J Endod. 2006 May;32(5):447-51. doi: 10.1016/j.joen.2005.10.061. Epub 2006 Feb 7.

Abstract

The influence of different silane/dentin adhesives on the microtensile bond strengths of a hybrid composite to sodium ethoxide-etched quartz fiber posts was investigated. A prehydrolyzed silane was applied without an adhesive and compared to two-component systems in which hydrolysis of the silane occurred after mixing with the acidic monomer present in the dentin adhesives. Nanoleakage along post/core interfaces was examined after silver nitrate tracer penetration using scanning electron microscopy. Higher interfacial strengths and more uniform adaptation between the etched fiber post surface and the composite core were recorded after post treatment with silane/adhesive couplings. The combination of silane with two-step self-etch adhesives improves the chemical retention of composites around etched fiber posts with minimal nanoleakage. Although the one-step self-etching adhesive/silane combination enhances post adhesion, the extensive nanoleakage provides channels for rapid water sorption that may expedite hydrolytic degradation of the post/core interface.

摘要

研究了不同硅烷/牙本质粘结剂对混合复合材料与乙醇钠蚀刻石英纤维桩微拉伸粘结强度的影响。应用了一种预水解硅烷,未使用粘结剂,并与两组分系统进行了比较,在两组分系统中,硅烷与牙本质粘结剂中存在的酸性单体混合后发生水解。使用扫描电子显微镜在硝酸银示踪剂渗透后检查桩/核界面的纳米渗漏情况。在用硅烷/粘结剂偶联剂处理桩后,记录到更高的界面强度以及蚀刻纤维桩表面与复合核之间更均匀的适配性。硅烷与两步自酸蚀粘结剂的组合提高了蚀刻纤维桩周围复合材料的化学固位力,纳米渗漏最小。尽管一步自酸蚀粘结剂/硅烷组合增强了桩的粘结力,但广泛的纳米渗漏提供了快速吸水的通道,这可能会加速桩/核界面的水解降解。

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