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不同固化模式和设备对可流动树脂复合材料微应变及转化率的影响。

Effects on microstrain and conversion of flowable resin composite using different curing modes and units.

作者信息

Tseng Wan-Yu, Chen Ruey-Song, Wang Jaw-Lin, Lee Ming-Shu, Rueggeberg Frederick A, Chen Min-Huey

机构信息

Graduate Institute of Clinical Dental Science, School of Dentistry, College of Medicine, National Taiwan University, Taipei, Taiwan.

出版信息

J Biomed Mater Res B Appl Biomater. 2007 May;81(2):323-9. doi: 10.1002/jbm.b.30668.

DOI:10.1002/jbm.b.30668
PMID:17022052
Abstract

The flowable resin composite, Tetric Flow, was used to measure microstrain and degree of conversion after hardening with each of three curing machines: XL3000(XL) for 10, 20, 30, and 40 s; Optilux 501 using conventional mode (OC) for 10, 20, 30, and 40 s, as well as Optilux boost (OB, 10 s) and ramp modes (OR, 20 s); and LEDemetron (LEDe) for 10, 20, 30, and 40 s. The emitted power density and spectral distribution of the three light curing units were also measured. The LEDe output energy spectrum was centralized between 425 and 490 nm, which encompasses the excited wavelength of camphorquinone. The microstrain produced by the curing process is as a second-degree polynomial for each light source. The OB microstrain was highest, while the OR microstrain was lower. The ranking in order of degree of monomer conversion was as follows: XL10 <or=<or= OC10 <or=<or= LED 10 = OR = XL 20 = OC 20 = XL 30 <or=<or= LED 20 <or=<or= OC30 = LED 40 = XL 40 = OC40 = LED 30 <or= OB. The degree of conversion cured with OB was significant higher than other curing modes except OC30, OC40, LEDe30, LEDe40, and XL40. The conversion value of XL10 was the lowest. The LEDe produced higher conversion for the same emitted energy compared to the two halogen units.

摘要

采用可流动树脂复合材料Tetric Flow,使用三种固化机分别固化后测量其微应变和固化转化率:XL3000(XL)固化10、20、30和40秒;Optilux 501采用传统模式(OC)固化10、20、30和40秒,以及Optilux增强模式(OB,10秒)和斜坡模式(OR,20秒);LEDemetron(LEDe)固化10、20、30和40秒。还测量了三种光固化单元的发射功率密度和光谱分布。LEDe的输出能谱集中在425至490纳米之间,该范围涵盖了樟脑醌的激发波长。固化过程产生的微应变对于每种光源均为二次多项式。OB产生的微应变最高,而OR产生的微应变较低。单体转化率的排序如下:XL10<或=OC10<或=LED 10 = OR = XL 20 = OC 20 = XL 30<或=LED 20<或=OC30 = LED 40 = XL 40 = OC40 = LED 30<或=OB。除OC30、OC40、LEDe30、LEDe40和XL40外,采用OB固化的转化率显著高于其他固化模式。XL10的转化率值最低。与两个卤素单元相比,对于相同的发射能量,LEDe产生的转化率更高。

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