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丙烯酸类可摘矫治器:不同后聚合方法的比较评估

Acrylic removable appliances: comparative evaluation of different postpolymerization methods.

作者信息

Faltermeier Andreas, Rosentritt Martin, Müssig Dieter

机构信息

Department of Orthodontics, University of Regensberg, Regensburg, Germany.

出版信息

Am J Orthod Dentofacial Orthop. 2007 Mar;131(3):301.e16-22. doi: 10.1016/j.ajodo.2006.07.019.

Abstract

INTRODUCTION

In orthodontics, the polymeric part of removable orthodontic appliances could be a hazard for patients because high residual monomer contents can lead to allergic reactions. In addition, water uptake, color stability, and mechanical properties are influenced by the degree of conversion. The aim of this investigation was to evaluate the effectiveness of different postpolymerization methods on the properties of removable orthodontic appliance resins.

METHODS

A total of 300 rectangular specimens (5 postpolymerization groups: 20 per group) were manufactured of Orthocryl (n = 100, Dentaurum, Ispringen, Germany), Palapress (n = 100, Heraeus-Kulzer, Wehrheim, Germany), and Pro Base Cold (n = 100, Ivoclar-Vivadent, Schaan, Liechtenstein). The first 2 postpolymerization groups were postcured in a stove (10 minutes at 40 degrees C or 80 degrees C). The third resin group was postcured in a microwave at 600W for 5 minutes, and the fourth polymer group was postcured in a microwave at 600W for 10 minutes. Twenty conventionally cured samples (cold-curing under pressure: water bath 40 degrees C, 25 minutes, 2.2 bar) were the control group. Water sorption, fracture toughness, and Vickers hardness were measured.

RESULTS

Fracture toughness and Vickers hardness of the resins are slightly increased after curing. Heat as a secondary curing method decreases water uptake of resins used for removable orthodontic appliances.

CONCLUSIONS

Heat postpolymerization appears to improve the properties of removable orthodontic appliance resins.

摘要

引言

在正畸学中,可摘正畸矫治器的聚合物部分可能对患者构成危害,因为高残留单体含量会导致过敏反应。此外,吸水率、颜色稳定性和机械性能会受到转化率的影响。本研究的目的是评估不同后聚合方法对可摘正畸矫治器树脂性能的有效性。

方法

共制作了300个矩形样本(5个后聚合组:每组20个),材料分别为Orthocryl(n = 100,德国伊施普林根的登泰克公司)、Palapress(n = 100,德国韦尔海姆的贺利氏古莎公司)和Pro Base Cold(n = 100,列支敦士登沙恩的义获嘉伟瓦登特公司)。前两个后聚合组在烘箱中后固化(40℃或80℃下10分钟)。第三组树脂在600W的微波炉中后固化5分钟,第四组聚合物在600W的微波炉中后固化10分钟。20个常规固化样本(压力下冷固化:40℃水浴,25分钟,2.2巴)作为对照组。测量了吸水率、断裂韧性和维氏硬度。

结果

固化后树脂的断裂韧性和维氏硬度略有增加。热作为二次固化方法可降低用于可摘正畸矫治器的树脂的吸水率。

结论

热后聚合似乎可改善可摘正畸矫治器树脂的性能。

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