Schlesiger Ralf, Oberdorfer Christian, Würz Roland, Greiwe Gerd, Stender Patrick, Artmeier Michael, Pelka Patrick, Spaleck Frank, Schmitz Guido
Institute of Material Physics, Westfälische Wilhelms-Universität, Wilhelm-Klemm-Str. 10, 48149 Münster, Germany.
Rev Sci Instrum. 2010 Apr;81(4):043703. doi: 10.1063/1.3378674.
To benefit from the latest technical improvements in atom probe analysis, a new tomographic atom probe has been built at the University of Münster, Germany. The instrument utilizes a femtosecond laser system with a high repetition rate combined with the ability of using a micrometer-sized extraction electrode and a wide angle configuration. Since field evaporation is triggered by laser pulses instead of high-voltage pulses, the instrument offers the ability to expand the range of analyzed materials to poorly conducting or insulating materials such as oxides, glasses, ceramics, and polymeric materials. The article describes the design of the instrument and presents characterizing measurements on metals, semiconductors, and oxide ceramic.
为了受益于原子探针分析的最新技术改进,德国明斯特大学建造了一台新的断层扫描原子探针。该仪器采用了具有高重复率的飞秒激光系统,并具备使用微米级提取电极和广角配置的能力。由于场蒸发是由激光脉冲而非高压脉冲触发的,该仪器能够将可分析材料的范围扩展到导电性差或绝缘的材料,如氧化物、玻璃、陶瓷和聚合物材料。本文描述了该仪器的设计,并展示了对金属、半导体和氧化物陶瓷的特性测量结果。