Watcharotone Supinda, Dikin Dmitriy A, Stankovich Sasha, Piner Richard, Jung Inhwa, Dommett Geoffrey H B, Evmenenko Guennadi, Wu Shang-En, Chen Shu-Fang, Liu Chuan-Pu, Nguyen SonBinh T, Ruoff Rodney S
Department of Mechanical Engineering, Northwestern University, Evanston, Illinois 60208, USA.
Nano Lett. 2007 Jul;7(7):1888-92. doi: 10.1021/nl070477+. Epub 2007 Jun 26.
Transparent and electrically conductive composite silica films were fabricated on glass and hydrophilic SiOx/silicon substrates by incorporation of individual graphene oxide sheets into silica sols followed by spin-coating, chemical reduction, and thermal curing. The resulting films were characterized by SEM, AFM, TEM, low-angle X-ray reflectivity, XPS, UV-vis spectroscopy, and electrical conductivity measurements. The electrical conductivity of the films compared favorably to those of composite thin films of carbon nanotubes in silica.
通过将单个氧化石墨烯片掺入硅溶胶中,随后进行旋涂、化学还原和热固化,在玻璃和亲水性氧化硅/硅衬底上制备了透明导电复合二氧化硅薄膜。通过扫描电子显微镜(SEM)、原子力显微镜(AFM)、透射电子显微镜(TEM)、低角度X射线反射率、X射线光电子能谱(XPS)、紫外可见光谱和电导率测量对所得薄膜进行了表征。与二氧化硅中碳纳米管复合薄膜相比,该薄膜的电导率表现良好。