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不同溶剂型粘合剂的湿粘结与干粘结的稳定性

Stability of wet versus dry bonding with different solvent-based adhesives.

作者信息

Manso Adriana P, Marquezini Luiz, Silva Safira M A, Pashley David H, Tay Franklyn R, Carvalho Ricardo M

机构信息

Department of Operative Dentistry, Endodontics and Dental Materials, Bauru School of Dentistry, University of São Paulo, Bauru, Brazil.

出版信息

Dent Mater. 2008 Apr;24(4):476-82. doi: 10.1016/j.dental.2007.04.009. Epub 2007 Aug 6.

Abstract

OBJECTIVE

To evaluate the effects of surface moisture (wet or dry) and storage (24h or 3 months) on the microtensile bond strength (BS) of resin/dentin bonds mediated by two water/ethanol based adhesives Single Bond, 3M-ESPE, (SB) and Opti Bond Solo Plus, Kerr, (OB), and two acetone-based adhesives, One Step, Bisco, (OS) and Prime&Bond NT, Caulk/Dentsply, (PB).

MATERIALS AND METHODS

Flat dentin surfaces were polished with 600-grit SiC paper, etched with 35% phosphoric acid for 15s and rinsed for 20s. Half the surface was maintained moist and the other half was air-dried for 30s. Each adhesive was applied simultaneously to both halves, left undisturbed for 30s and light-cured. Four-mm resin build-ups were constructed incrementally. After storage in water at 37 degrees C for 24h, slabs were produced by transversal sectioning and trimmed to an hourglass shape (0.8mm2). Half of the specimens were tested in tension at 0.6mm/min immediately after trimming and the other half after 3 months of water storage. Data were analyzed by two-way ANOVA and SNK for each material.

RESULTS

Both moisture and storage affected BS to dentin, and was material-dependent. Dry bonding affected mostly the acetone-based adhesives. Larger reductions in bond strength were associated with dry bonding after 3 months of water storage.

SIGNIFICANCE

Wet bonding resulted in more stable bonds over 3 months of water storage for most of the materials tested.

摘要

目的

评估表面湿度(湿或干)和储存条件(24小时或3个月)对两种水/乙醇基粘合剂(3M-ESPE公司的Single Bond(SB)和Kerr公司的Opti Bond Solo Plus(OB))以及两种丙酮基粘合剂(Bisco公司的One Step(OS)和Caulk/Dentsply公司的Prime&Bond NT(PB))介导的树脂/牙本质粘结微拉伸粘结强度(BS)的影响。

材料与方法

用600目碳化硅砂纸打磨平坦的牙本质表面,用35%磷酸蚀刻15秒,冲洗20秒。将一半表面保持湿润,另一半风干30秒。将每种粘合剂同时应用于两半表面,静置30秒后光固化。逐层构建4毫米厚的树脂堆积物。在37℃水中储存24小时后,通过横向切片制作薄片,并修剪成沙漏形状(0.8平方毫米)。一半标本在修剪后立即以0.6毫米/分钟的速度进行拉伸测试,另一半在水储存3个月后进行测试。对每种材料的数据进行双向方差分析和SNK分析。

结果

湿度和储存均影响与牙本质的粘结强度,且与材料有关。干式粘结主要影响丙酮基粘合剂。水储存3个月后,干式粘结导致的粘结强度降低幅度更大。

意义

对于大多数测试材料,湿式粘结在水储存3个月期间能产生更稳定的粘结。

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