Hanrahan Grady, Tse Florence, Dahdouh Froseen T, Clarke Keith, Gomez Frank A
Department of Chemistry & Biochemistry, California State University, Los Angeles, CA 90032, USA.
J Capill Electrophor Microchip Technol. 2007;10(1-2):1-6.
The development and experimental optimization of a novel flow injection-capillary electrophoresis (FI-CE) analyzer employing UV-visible fiber optic detection is described. The analyzer incorporates a miniature charge-coupled device (CCD) spectrometer and operates in a graphical programming environment. Data from experimental optimization studies and small molecule separations involving affinity capillary electrophoresis (ACE) and indirect detection of anions are presented. Future directions in terms of instrument automation and incorporation into a microfluidic format are also discussed.
描述了一种采用紫外-可见光纤检测的新型流动注射-毛细管电泳（FI-CE）分析仪的开发及实验优化。该分析仪集成了微型电荷耦合器件（CCD）光谱仪，并在图形化编程环境中运行。展示了来自实验优化研究以及涉及亲和毛细管电泳（ACE）和阴离子间接检测的小分子分离的数据。还讨论了仪器自动化以及纳入微流控形式方面的未来发展方向。
