Loyaga-Rendon Paola G, Takahashi Hidekazu, Hayakawa Iwao, Iwasaki Naohiko
Division of Oral Health Sciences, Graduate School, Tokyo Medical and Dental University, Tokyo, Japan.
J Prosthet Dent. 2007 Aug;98(2):141-9. doi: 10.1016/S0022-3913(07)60047-X.
New types of artificial teeth are commercially available; however, evidence-based information regarding composition and properties is lacking.
The purpose of this study was to qualify the compositional characteristics and hardness of new commercially available types of acrylic resin and composite resin artificial teeth.
Twelve brands of 3 types (2 conventional acrylic resins, 3 cross-linked acrylic resins, and 7 composite resins) of artificial teeth were examined. The filler geometry and composition were observed using scanning electron microscopy and energy disperse x-ray analysis, respectively. Vickers hardness was determined for each layer of the polished cross-sectioned teeth. The inorganic content of the enamel layer was determined by thermogravimetric analysis with an ash method. The swelling behavior of the artificial teeth after 12 hours of methyl methacrylate immersion was observed to determine the cross-linking structure. The data were statistically analyzed using 1-way analysis of variance and Tukey's multiple comparison (alpha=.05).
Examined teeth were composed of 2, 3, or 4 layers of resin. Different sizes and shapes of filler were found but were composed only of silicon oxide. Vickers hardness ranged from 17.4 to 47.0 kgf/mm(2). The inorganic content ranged from 0 to 42.8 mass%. The enamel layer of all teeth, except for 3 products, produced negligible swelling, and the base layer of all the teeth, except for 2 products, produced obvious swelling. A significant linear correlation was observed between hardness and inorganic content.
Within the limitations of this study, differences in size, shape, distribution, and content of the silica filler and the cross-linking nature of the resin matrix were found among the commercial brands of artificial teeth evaluated.
新型人造牙已投放市场;然而,关于其成分和性能的循证信息却很缺乏。
本研究旨在鉴定新型市售丙烯酸树脂和复合树脂人造牙的成分特征及硬度。
对3种类型(2种传统丙烯酸树脂、3种交联丙烯酸树脂和7种复合树脂)的12个品牌的人造牙进行了检测。分别使用扫描电子显微镜和能量色散X射线分析观察填料的几何形状和成分。测定了经抛光的牙齿横截面各层的维氏硬度。采用灰化法通过热重分析测定釉质层的无机含量。观察人造牙在甲基丙烯酸甲酯中浸泡12小时后的溶胀行为,以确定交联结构。数据采用单因素方差分析和Tukey多重比较进行统计学分析(α = 0.05)。
检测的牙齿由2、3或4层树脂组成。发现填料有不同的尺寸和形状,但仅由氧化硅组成。维氏硬度范围为17.4至47.0 kgf/mm²。无机含量范围为0至42.8质量%。除3种产品外,所有牙齿的釉质层溶胀可忽略不计;除2种产品外,所有牙齿的基底层溶胀明显。硬度与无机含量之间存在显著的线性相关性。
在本研究的局限性范围内,在所评估的人造牙商业品牌中,发现二氧化硅填料的尺寸、形状、分布和含量以及树脂基质的交联性质存在差异。