Bondu Stéphanie, Kervarec Nelly, Deslandes Eric, Pichon Roger
Institut Universitaire Européen de la Mer, Université de Bretagne Occidentale, Technopôle de Brest-Iroise, F-29280 Plouzané, France.
Carbohydr Res. 2007 Nov 26;342(16):2470-3. doi: 10.1016/j.carres.2007.07.021. Epub 2007 Aug 6.
Isofloridosides (1-O-alpha-D-galactopyranosylglycerol) and floridoside (2-O-alpha-D-galactopyranosylglycerol) were extracted from the red alga Porphyra umbilicalis (Linné) Kützing (Bangiales, Rhodophyta). Their separation was achieved by HPLC (NH(2) P50 column) after successive purification of the crude extract by ion-exchange chromatography and HPLC (Sugar-Pak TM1 column). 1D and 2D NMR spectroscopy experiments allowed to completely assign the (1)H and (13)C spectra of D-isofloridoside.
异弗罗里糖苷（1-O-α-D-吡喃半乳糖基甘油）和弗罗里糖苷（2-O-α-D-吡喃半乳糖基甘油）是从红藻紫菜（林奈）库茨（红毛菜纲，红藻门）中提取的。在通过离子交换色谱法和高效液相色谱法（Sugar-Pak TM1柱）对粗提取物进行连续纯化后，通过高效液相色谱法（NH(2) P50柱）实现了它们的分离。一维和二维核磁共振光谱实验能够完全确定D-异弗罗里糖苷的氢谱和碳谱。
