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Solid-state protein-structure determination with proton-detected triple-resonance 3D magic-angle-spinning NMR spectroscopy.

作者信息

Zhou Donghua H, Shea John J, Nieuwkoop Andrew J, Franks W Trent, Wylie Benjamin J, Mullen Charles, Sandoz Dennis, Rienstra Chad M

机构信息

Department of Chemistry, University of Illinois at Urbana-Champaign, Urbana, IL 61801, USA.

出版信息

Angew Chem Int Ed Engl. 2007;46(44):8380-3. doi: 10.1002/anie.200702905.

DOI:10.1002/anie.200702905
PMID:17907259
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2790053/
Abstract
摘要

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本文引用的文献

1
Proton-detected solid-state NMR spectroscopy of fully protonated proteins at 40 kHz magic-angle spinning.在40千赫兹魔角旋转条件下对完全质子化蛋白质进行质子检测的固态核磁共振光谱学。
J Am Chem Soc. 2007 Sep 26;129(38):11791-801. doi: 10.1021/ja073462m. Epub 2007 Aug 29.
2
Observation of heteronuclear overhauser effects confirms the 15N-1H dipolar relaxation mechanism in a crystalline protein.异核Overhauser效应的观察证实了晶体蛋白中的15N-1H偶极弛豫机制。
J Am Chem Soc. 2006 Sep 27;128(38):12398-9. doi: 10.1021/ja064037g.
3
Ultrahigh resolution in proton solid-state NMR spectroscopy at high levels of deuteration.高氘代水平下质子固态核磁共振光谱中的超高分辨率。
Angew Chem Int Ed Engl. 2006 Jun 2;45(23):3878-81. doi: 10.1002/anie.200600328.
4
SOLARIA: a protocol for automated cross-peak assignment and structure calculation for solid-state magic-angle spinning NMR spectroscopy.SOLARIA：一种用于固态魔角旋转核磁共振光谱的自动交叉峰归属和结构计算的协议。
Angew Chem Int Ed Engl. 2005 Sep 26;44(38):6151-4. doi: 10.1002/anie.200501884.
5
Magic-angle spinning solid-state NMR spectroscopy of the beta1 immunoglobulin binding domain of protein G (GB1): 15N and 13C chemical shift assignments and conformational analysis.蛋白质G（GB1）的β1免疫球蛋白结合结构域的魔角旋转固态核磁共振光谱：15N和13C化学位移归属及构象分析
J Am Chem Soc. 2005 Sep 7;127(35):12291-305. doi: 10.1021/ja044497e.
6
A concept for rapid protein-structure determination by solid-state NMR spectroscopy.一种通过固态核磁共振光谱快速测定蛋白质结构的概念。
Angew Chem Int Ed Engl. 2005 Mar 29;44(14):2089-92. doi: 10.1002/anie.200462516.
7
Reduction of RF-induced sample heating with a scroll coil resonator structure for solid-state NMR probes.用于固态核磁共振探头的涡旋线圈谐振器结构减少射频感应样品加热
J Magn Reson. 2005 Mar;173(1):40-8. doi: 10.1016/j.jmr.2004.11.015.
8
Sensitive high resolution inverse detection NMR spectroscopy of proteins in the solid state.固态蛋白质的灵敏高分辨率反向检测核磁共振光谱法。
J Am Chem Soc. 2003 Dec 24;125(51):15831-6. doi: 10.1021/ja037315+.
9
High-sensitivity observation of dipolar exchange and NOEs between exchangeable protons in proteins by 3D solid-state NMR spectroscopy.通过三维固态核磁共振光谱对蛋白质中可交换质子之间的偶极交换和核Overhauser效应进行高灵敏度观测。
J Am Chem Soc. 2003 Nov 26;125(47):14222-3. doi: 10.1021/ja037559u.
10
Water-protein interactions in microcrystalline crh measured by 1H-13C solid-state NMR spectroscopy.通过1H-13C固态核磁共振光谱法测量微晶状CRH中的水-蛋白质相互作用。
J Am Chem Soc. 2003 Nov 5;125(44):13336-7. doi: 10.1021/ja036720y.