Solid-state protein-structure determination with proton-detected triple-resonance 3D magic-angle-spinning NMR spectroscopy.
作者信息
Zhou Donghua H, Shea John J, Nieuwkoop Andrew J, Franks W Trent, Wylie Benjamin J, Mullen Charles, Sandoz Dennis, Rienstra Chad M
机构信息
Department of Chemistry, University of Illinois at Urbana-Champaign, Urbana, IL 61801, USA.
出版信息
Angew Chem Int Ed Engl. 2007;46(44):8380-3. doi: 10.1002/anie.200702905.
Abstract
摘要
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本文引用的文献
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Proton-detected solid-state NMR spectroscopy of fully protonated proteins at 40 kHz magic-angle spinning.在40千赫兹魔角旋转条件下对完全质子化蛋白质进行质子检测的固态核磁共振光谱学。
J Am Chem Soc. 2007 Sep 26;129(38):11791-801. doi: 10.1021/ja073462m. Epub 2007 Aug 29.
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Observation of heteronuclear overhauser effects confirms the 15N-1H dipolar relaxation mechanism in a crystalline protein.异核Overhauser效应的观察证实了晶体蛋白中的15N-1H偶极弛豫机制。
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Ultrahigh resolution in proton solid-state NMR spectroscopy at high levels of deuteration.高氘代水平下质子固态核磁共振光谱中的超高分辨率。
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J Am Chem Soc. 2005 Sep 7;127(35):12291-305. doi: 10.1021/ja044497e.
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A concept for rapid protein-structure determination by solid-state NMR spectroscopy.一种通过固态核磁共振光谱快速测定蛋白质结构的概念。
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Reduction of RF-induced sample heating with a scroll coil resonator structure for solid-state NMR probes.用于固态核磁共振探头的涡旋线圈谐振器结构减少射频感应样品加热
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Sensitive high resolution inverse detection NMR spectroscopy of proteins in the solid state.固态蛋白质的灵敏高分辨率反向检测核磁共振光谱法。
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