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在Ti-6Al-4V和316L不锈钢植入材料上进行生物陶瓷浸涂。

Bioceramic dip-coating on Ti-6Al-4V and 316L SS implant materials.

作者信息

Aksakal Bunyamin, Hanyaloglu C

机构信息

Department of Mechanical Education, Faculty of Technical Education, Firat University, Elazig, Turkey.

出版信息

J Mater Sci Mater Med. 2008 May;19(5):2097-104. doi: 10.1007/s10856-007-3304-2. Epub 2007 Oct 30.

Abstract

The focus of the present study is based on more economical and rapid bioceramic coating on the most common implant substrates such as Ti-6Al-4V and 316L SS used often in orthopedics. For ceramic dip coating of implant substrates, Hydroxyapatite (HA) powder, Ca10(PO4)6(OH)2, P2O5, Na2CO3 and KH2PO4 are used to provide the gel. Ceramic films on sandblasted substrates have been deposited by using a newly manufactured dip-coating apparatus. Sample characterization is evaluated by SEM and XRD analysis. A smooth and homogeneous coating films have been obtained and average of 20 MPa bonding strength has been achieved for both Ti-6Al-4V and 316L SS alloys after sintering at 750 degrees C under flowing argon. The level of importance of the process parameters on coating was determined by using analysis of variance (ANOVA). The current process appears to be cheap, easy, and flexible to shape variations and high production rates for orthopedic applications.

摘要

本研究的重点是在骨科中常用的最常见植入基体(如Ti-6Al-4V和316L不锈钢)上制备更经济、快速的生物陶瓷涂层。对于植入基体的陶瓷浸涂,使用羟基磷灰石(HA)粉末、Ca10(PO4)6(OH)2、P2O5、Na2CO3和KH2PO4来制备凝胶。通过使用新制造的浸涂设备,在喷砂处理的基体上沉积陶瓷膜。通过扫描电子显微镜(SEM)和X射线衍射(XRD)分析对样品进行表征。已获得光滑且均匀的涂层膜,在750℃流动氩气中烧结后,Ti-6Al-4V和316L不锈钢合金均实现了平均20MPa的结合强度。通过方差分析(ANOVA)确定了工艺参数对涂层的重要程度。目前的工艺似乎成本低廉、操作简便,并且对于形状变化具有灵活性,适用于骨科应用的高生产率。

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