Krivanek O L, Corbin G J, Dellby N, Elston B F, Keyse R J, Murfitt M F, Own C S, Szilagyi Z S, Woodruff J W
Nion Co., 1102 8th Street, Kirkland, WA 98033, USA.
Ultramicroscopy. 2008 Feb;108(3):179-95. doi: 10.1016/j.ultramic.2007.07.010. Epub 2007 Oct 22.
Improved resolution made possible by aberration correction has greatly increased the demands on the performance of all parts of high-end electron microscopes. In order to meet these demands, we have designed and built an entirely new scanning transmission electron microscope (STEM). The microscope includes a flexible illumination system that allows the properties of its probe to be changed on-the-fly, a third-generation aberration corrector which corrects all geometric aberrations up to fifth order, an ultra-responsive yet stable five-axis sample stage, and a flexible configuration of optimized detectors. The microscope features many innovations, such as a modular column assembled from building blocks that can be stacked in almost any order, in situ storage and cleaning facilities for up to five samples, computer-controlled loading of samples into the column, and self-diagnosing electronics. The microscope construction is described, and examples of its capabilities are shown.
像差校正带来的分辨率提升极大地增加了对高端电子显微镜各部件性能的要求。为了满足这些要求,我们设计并制造了一台全新的扫描透射电子显微镜(STEM)。该显微镜包括一个灵活的照明系统,可随时改变其探针特性;一个第三代像差校正器,可校正直至五阶的所有几何像差;一个超灵敏且稳定的五轴样品台,以及一组灵活配置的优化探测器。该显微镜有许多创新之处,比如由可按几乎任何顺序堆叠的模块构建而成的模块化镜筒、用于多达五个样品的原位存储和清洁设施、计算机控制的样品加载到镜筒过程以及具有自诊断功能的电子设备。本文描述了显微镜的构造,并展示了其功能示例。