Sauter A M, Wartburg J P
J Chromatogr. 1977 Mar 11;133(1):167-72. doi: 10.1016/s0021-9673(00)89217-1.
A simple method is described that permits the direct quantitative determination of carbon disulphide, free diethyldithiocarbamate and disulphides derived from disulfiram in 1 ml of a patient's blood. It is based on a gas chromatographic determination of carbon disulphide produced from diethyldithiocarbamate and disulfiram using the head-space technique and a flame-photometric detector. The method is compared with a recently described spectrophotometric method.
本文描述了一种简单的方法，可直接定量测定患者1毫升血液中的二硫化碳、游离二乙基二硫代氨基甲酸盐以及由双硫仑衍生而来的二硫化物。该方法基于采用顶空技术和火焰光度检测器对二乙基二硫代氨基甲酸盐和双硫仑产生的二硫化碳进行气相色谱测定。将该方法与最近描述的分光光度法进行了比较。
