Raabe J, Tzvetkov G, Flechsig U, Böge M, Jaggi A, Sarafimov B, Vernooij M G C, Huthwelker T, Ade H, Kilcoyne D, Tyliszczak T, Fink R H, Quitmann C
Swiss Light Source, Paul Scherrer Institut, Villigen-PSI, Switzerland.
Rev Sci Instrum. 2008 Nov;79(11):113704. doi: 10.1063/1.3021472.
We report on the successful installation and operation of a scanning transmission x-ray microspectroscope (STXM) at the PolLux facility at the Swiss Light Source. This integration of an advanced STXM with improved sample handling capabilities and a novel beamline provides unique capabilities. PolLux uses linearly or circularly polarized x-rays from a bending magnet with an extended photon energy range (200-1400 eV). It is therefore well suited to determine a sample's quantitative chemical composition, molecular orientation, or thickness of organic as well as condensed matter materials. The local magnetic state of magnetic thin films is accessible through fast helicity switching by steering the electron beam off axis through the bending magnet. Ex vacuo girder movers allow fast and highly reproducible (<1 microm) alignment of the instrument with respect to the photon beam. The present spatial resolution is approximately 20 nm, limited by the zone plates utilized. The instrument has the stability and positional resolution to operate with much higher resolution optics as it becomes available. In addition to characterization experiments, we present several typical examples from materials research and environmental science to exemplify the capabilities.
我们报告了在瑞士光源的PolLux装置上成功安装并运行扫描透射X射线显微镜(STXM)的情况。这种将先进的STXM与改进的样品处理能力和新型光束线相结合的方式提供了独特的功能。PolLux使用来自弯曲磁铁的线偏振或圆偏振X射线,其光子能量范围较宽(200 - 1400 eV)。因此,它非常适合确定有机材料以及凝聚态物质材料的定量化学成分、分子取向或厚度。通过使电子束偏离轴穿过弯曲磁铁进行快速螺旋度切换,可以获取磁性薄膜的局部磁状态。真空梁式移动器能够实现仪器相对于光子束的快速且高度可重复(<1微米)的对准。目前的空间分辨率约为20纳米,受所用波带片的限制。随着更高分辨率光学元件的出现,该仪器具备以更高分辨率运行的稳定性和位置分辨率。除了表征实验外,我们还展示了材料研究和环境科学中的几个典型例子,以说明其功能。